Structural investigations of azithromycin , its derivatives and copper complex

Kamenar, B.; Košutić-Hulita, Nada; Mrvoš-Sermek, Draginja; Nagl, Ante; Vicković, I.; Ðokić, Slobodan; Kobrehel, Gabrijela; Lazarevski, Gorjana; Lopotar, Nevenka; Vinković, Mladen; Metelko, Biserka; Vikić‐Topić, Dražen

doi:10.1107/s0108767378096312

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1994

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“…About 30 years ago in a short conference note, Kamenar (1963) reported that lead(IV) acetate, Pb(Omc)4 (OAc = CH3COO), crystallizes in space group P21/c with Z = 8, the structure consisting of two symmetrically independent sets of molecules. The polyhedron around the eightcoordinate Pb atom was described as a flattened trigonal dodecahedron.…”

Section: Commentmentioning

confidence: 99%

“…Apart from the cell dimensions [a = 13.01 (2), b = 26.59 (4), c = 7.86 (2) ]k, [3 = 105.6 (2)°], no other data were given. A full description was announced after due refinement of the atomic coordinates (Kamenar, 1963;Kamenar & Bruvo, 1972), but to our knowledge it was not published. Since our studies on organolead(IV) carboxylates would profit from detailed structural data of Pb(OAc)4, (I), we have redetermined the structure of this compound.…”

Section: Commentmentioning

confidence: 99%

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