Structural Diversity Design, Four Nucleation Methods Growth and Mechanism of 3D Hollow Box TiO2 Nanocrystals with a Temperature-Controlled High (001) Crystal Facets Exposure Ratio
Shengqiang Liao,
Huan Liu,
Yanfei Lu
et al.
Abstract:Three-dimensional
(3D) hollow box TiO2 nanocrystals
with structural diversity have been designed and grown by four nucleation
methods, including the acid dissolution denucleation method with Fe2O3 as heterogeneous nucleation, the topological
phase transition method, the sonic solvothermal method, and the air
atmosphere sintering method with TiOF2 as homogeneous nucleation.
Through full morphology analysis and structural characterization,
reasonable growth mechanisms of 3D hollow box TiO2 nanocrystals
were prop… Show more
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