Abstract:Yucca fiber is a natural cellulose fiber that can be extracted from the Yucca plant leaves by retting. The physical properties of the Yucca fiber are extremely sensitive to the retting conditions. This research was designed to study the effects of chemical retting on the structural and properties of this fiber. Chemical retting was done by soaking the Yucca leaf in 10 to 150 g/l sodium hydroxide concentration at 80 to 100 °C for 60 to 240 min. Fiber characteristics such as fineness, tenacity, functional groups… Show more
“…The resultant slightly higher fiber's crystallinity in Table 4 was due to the partial removal of non‐crystalline materials such as external lignin and hemicellulose. As a comparison, recent studies reported the fiber crystallinity of agave Yucca ( Asparagus ) up to 66%, depending on the temperature of chemical extraction 32 . In another report, the crystallinity of Yucca ( Aloifolia ) leaves calculated by the Segal method was 69.43% 33 .…”
Section: Resultsmentioning
confidence: 95%
“…As a comparison, recent studies reported the fiber crystallinity of agave Yucca (Asparagus) up to 66%, depending on the temperature of chemical extraction. 32 In another report, the crystallinity of Yucca (Aloifolia) leaves calculated by the Segal method was 69.43%. 33 These results indicate that fibers obtained from branches of Yucca (Asparageae) have lower crystallinity than agave-like fibers.…”
The preparation and characterization of Yucca Filifera (Asparagaceae) fibers (YFF) and their incorporation into polypropylene (PP) matrices of two molecular weights are reported. Apart from the fibers sectioning and dehydration, saponates, phenols, hemicellulose, and lignin were systematically extracted. Moisture was a primary factor in the as‐sectioned samples, and dehydration was followed by volatiles extraction, including saponates and phenols. An optimized mixture of alcohols (80% methanol/20% ethanol v/v) was used to extract the remaining volatiles (adsorbed water, phenols, and saponates). The dried fibers were then cyclically treated in an autoclave using a dilute sodium hydroxide (NaOH) with the purpose of decreasing external lignin and hemicellulose. After extractions, the fiber product was directly incorporated into PP of two molecular weights, film/fiber (PP35) and injection molding (PP11) grades. The average crystallization temperatures from the melt increased slightly in the presence of YFF as an indication of heterogeneous nucleation. Although the crystallization degree decreased perceptibly depending on the fiber content. The apparent viscosity measurements as a function of shear rate, at low fiber concentrations (10 wt%), displayed partial compatibility between the treated YFF and PP11. In contrast, high fiber concentrations (30 wt%) in PP35 showed only a range of partial compatibility at high shear rates. Mechanical elongation and bending demonstrated an increase in the corresponding moduli as an indication of fiber reinforcement with a biodegradable additive. The higher tensile modulus was obtained at the expense of mechanical deformation.Highlights
A desert plant fiber works as reinforcement for PP composites.
The fibers preparation extracts saponates, phenols, and partially lignin and hemicellulose.
Fibers are heterogeneous enough for compatibility with the PP matrices.
Fibers mechanically reinforced PP in proportion to their concentration.
Reinforcement depends on the molecular weight of the PP matrix.
“…The resultant slightly higher fiber's crystallinity in Table 4 was due to the partial removal of non‐crystalline materials such as external lignin and hemicellulose. As a comparison, recent studies reported the fiber crystallinity of agave Yucca ( Asparagus ) up to 66%, depending on the temperature of chemical extraction 32 . In another report, the crystallinity of Yucca ( Aloifolia ) leaves calculated by the Segal method was 69.43% 33 .…”
Section: Resultsmentioning
confidence: 95%
“…As a comparison, recent studies reported the fiber crystallinity of agave Yucca (Asparagus) up to 66%, depending on the temperature of chemical extraction. 32 In another report, the crystallinity of Yucca (Aloifolia) leaves calculated by the Segal method was 69.43%. 33 These results indicate that fibers obtained from branches of Yucca (Asparageae) have lower crystallinity than agave-like fibers.…”
The preparation and characterization of Yucca Filifera (Asparagaceae) fibers (YFF) and their incorporation into polypropylene (PP) matrices of two molecular weights are reported. Apart from the fibers sectioning and dehydration, saponates, phenols, hemicellulose, and lignin were systematically extracted. Moisture was a primary factor in the as‐sectioned samples, and dehydration was followed by volatiles extraction, including saponates and phenols. An optimized mixture of alcohols (80% methanol/20% ethanol v/v) was used to extract the remaining volatiles (adsorbed water, phenols, and saponates). The dried fibers were then cyclically treated in an autoclave using a dilute sodium hydroxide (NaOH) with the purpose of decreasing external lignin and hemicellulose. After extractions, the fiber product was directly incorporated into PP of two molecular weights, film/fiber (PP35) and injection molding (PP11) grades. The average crystallization temperatures from the melt increased slightly in the presence of YFF as an indication of heterogeneous nucleation. Although the crystallization degree decreased perceptibly depending on the fiber content. The apparent viscosity measurements as a function of shear rate, at low fiber concentrations (10 wt%), displayed partial compatibility between the treated YFF and PP11. In contrast, high fiber concentrations (30 wt%) in PP35 showed only a range of partial compatibility at high shear rates. Mechanical elongation and bending demonstrated an increase in the corresponding moduli as an indication of fiber reinforcement with a biodegradable additive. The higher tensile modulus was obtained at the expense of mechanical deformation.Highlights
A desert plant fiber works as reinforcement for PP composites.
The fibers preparation extracts saponates, phenols, and partially lignin and hemicellulose.
Fibers are heterogeneous enough for compatibility with the PP matrices.
Fibers mechanically reinforced PP in proportion to their concentration.
Reinforcement depends on the molecular weight of the PP matrix.
“…The crystal size of the BPF was 5.22 nm. This smaller crystal size made the BPF more chemically reactive and water-soluble, which might improve the dyeing of these fibres (18) .…”
Section: Results Of Xrd Analysismentioning
confidence: 99%
“…The C = C aromatic ring and C-H vibration of lignin were associated with the peak at 1640 cm -1 , whereas the C-H deformation of cellulose and lignin was associated with the peak at 1384 cm -1 . In addition, a peak at 1034 cm -1 shows the existence of the C-H rocking vibration in cellulose (18) .…”
Objectives: A novel natural cellulose bismarck palm fibre (BPF) has been discovered and extracted from the leaf stalk of its tree. Physical, chemical, mechanical, and thermal characterizations have been conducted in this current study. Methods: A water retting method was employed for the extraction of BPFs. The diameter of BPF was assessed using an optical microscope image analyzer. A single fibre tensile test method was employed to calculate the tensile strength of BPF. The thermal behaviour of BPF was evaluated using thermo gravimetric analysis (TGA). A scanning electron microscope was utilized to evaluate the surface morphological structure of the BPF. Findings: The BPF has a fibre fineness of 819 denier, a mean diameter of 0.3636 mm, a density of 0.98 g/cc, cellulose content of 70.71%, hemi cellulose of 34.89%, lignin of 12.88%, wax of 0.30%, ash of 2.13 %, moisture of 10.80 %, pectin of 3.08 %, a mean breaking tensile strength of 904 MPa, mean breaking elongation of 6.4 %, and Young's modulus of 28.6 GPa, respectively. It is evident that the thermal analysis of BPF was thermally sustainable up to 268 • C. The results ensure that the BPF is the anticipated reinforcement of fibre-reinforced composite materials. SEM images revealed that cross section of BPF sample and rugged surface along the length of the fibre. Novelty: The higher cellulose percentage content of BPF samples has significantly shown better mechanical behaviour and thermal stability. This characterization evidenced that it is an outstanding alternative natural cellulose fibre for Eleusine indica grass fibres, Saccharum Bengalense fibres, Leucas Aspera fibres, Catharanthus roseus fibres, and Tridax procumbens fibres and also for synthetic fibres.
“…Some fibers, potentially suitable for incorporation into composites, are obtained from the leaves of plants that belong to the former Agavaceae family. This is the case for Agave americana , where natural retting, possibly followed by chemical treatment, proved effective for the production of composites (Hulle et al 2015; Madhu et al 2020; Murugesan et al 2022), and for Yucca filamentosa , where ambitions to obtain possible textile products from short fiber winding were also exposed (Nair et al 2013; Moghaddam and Karimi 2022). As far as the Sansevieria genus is concerned, three types offered fibers that might be used for the production of composites, namely Sansevieria trifasciata (Adeniyi et al 2020), Sansevieria ehrenbergii (Sathishkumar et al 2013), and particularly Sansevieria cylindrica (Sreenivasan et al 2015), in which a larger number of studies on the fibers has been carried out.…”
A number of natural fibers are being proposed for use in composite materials, especially those extracted from local plants, especially those able to grow spontaneously as they are cost‐efficient and have unexplored potential. Sansevieria cylindrica, within the Asparagaceae (previously Agavacae) family, has recently been considered for application in polymer and rubber matrix composites. However, its characterization and even the sorting out of technical fiber from the stem remains scarce, with little available data, as is often the case when the fabrication of textiles is not involved. In this study, Sansevieria cylindrica fibers were separated down to the dimensions of a filament at an 8–15 micron diameter from the stem of the plant, then characterized physically and chemically, using Fourier transform infrared spectroscopy (FTIR), morphologically by scanning electron microscopy (SEM), as well as their thermal degradation, by thermogravimetric analysis (TGA). Their crystallinity surface roughness was measured by X‐ray diffraction (XRD) and atomic force microscopy (AFM), respectively. The results indicate over 70% cellulose fibers content with a very high crystallinity (92%) and small crystallite size (1.45 nm), which suggests a low water absorption, with thermal degradation peaking at 294°C. Despite this, due to the significant porosity of the cellular structure, the density of 1.06 g cm−3 is quite low for a mainly cellulose fiber. Roughness measurements indicate that the porosities and foamy structure result in a highly negative skewness (−3.953), in the presence of deep valleys, which may contribute to an effective relation with a covering resin.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.