Stereoisomerization of the Ṗ(OCH2CH2)3N+BF4–radical: a single-crystal e.s.r. study

Hamerlinck, Joep H. H.; Schipper, Pieter E.; Buck, HM Henk

doi:10.1039/c39810001148

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“…Comparison of the isotropic and anisotropic phosphorus hfc for the CzV and CgV radicals of PI-& and PF, indicate that their magnitude is comparable for both isomers of the &I,, and PF4 radical respectively. The same result was experimentally demonstrated by Hamerlinck et al [22,231 in a sin le c stal ESR study of the TBP-e (C,,) and TBP-a (Cj,) isomers of eBF4 radical. the l (OCZH4) 3 The calculations predict larger hfc for the CaV isomers, whereas the reverse was found experimentally (Fig.…”

Section: Discussionsupporting

confidence: 72%