“…IR (neat): 3078, 2961, 2917, 2851, 1644, 1513, 1250, 1091, 1040: δ = 7.24 (d, J = 8. 6 Hz, 2 H, Ar), 6.86 (d,J = 8.6 Hz,2 H,Ar),4.79 (s,1 H,C=CH),4.74 (s,1 H,C=CH),1 H,TMSOC=CH),4.42 (d,J = 11.7 Hz,1 H,CH 2 Ar),4.34 (d,J = 11.7 Hz,1 H,CH 2 Ar), 3.80 (s,3 H,OCH 3 ),3 H,CH 2 OPMB,CHC=C),2.36 (pent,J = 6.8 Hz,1 H,CHMe),2.21 (pent,J = 7.2 Hz,1 H,CHCOPMB),1.68 (s,3 H,C=CCH 3 ), 1.08 (d,J = 6.8 Hz,3 H,CH 3 ),0.22 (s,9 H,TMS). 13 C NMR (50 MHz, CDCl 3 ): δ = 159.…”