2023
DOI: 10.12688/openreseurope.15699.1
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Standard Operating Procedure for the analysis of trace elements in hydrothermal fluids by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)

Abstract: This standard operating procedure (SOP) validates an inductively coupled plasma mass spectrometry (ICP-MS) procedure for the trace element determinations in hydrothermal fluids. Hydrothermal fluids are aqueous solutions with a wide range of temperature, salinity, pH and trace elements that can be used by a set of microbial proteins containing redox-sensitive transition metals as their catalytic core. Due to the high variability of these samples, we have developed this protocol taking into account the special f… Show more

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“…We measured the exact concentrations of cobalt (Co), nickel (Ni), iron (Fe), manganese (Mn), and copper (Cu) according to the method combining the isotope dilution with standard additions [ 29 ] and using the Agilent inductively coupled plasma mass spectrometer (ICP-MS7700x). The Quality Assurance/Quality Control (QA/QC) procedures followed PARCC principles, including precision, accuracy, representativeness, completeness, and comparability [ 30 ].…”
Section: Methodsmentioning
confidence: 99%
“…We measured the exact concentrations of cobalt (Co), nickel (Ni), iron (Fe), manganese (Mn), and copper (Cu) according to the method combining the isotope dilution with standard additions [ 29 ] and using the Agilent inductively coupled plasma mass spectrometer (ICP-MS7700x). The Quality Assurance/Quality Control (QA/QC) procedures followed PARCC principles, including precision, accuracy, representativeness, completeness, and comparability [ 30 ].…”
Section: Methodsmentioning
confidence: 99%