SRF material research using muon spin rotation and beta-detected nuclear magnetic resonance

Abstract

Muon spins precess in transverse magnetic fields and emit a positron preferentially in the spin direction at the instant of decay, enabling muon spin rotation (μSR) as a precise probe of local magnetic fields in matter. μSR has been used to characterize superconducting radio-frequency (SRF) materials since 2010. At TRIUMF, a beam of 4.2 MeV μ+ is implanted at a material-dependent depth of approximately 150 μm. A dedicated spectrometer was developed to measure the field of first vortex penetration and pinning strength in SRF materials in parallel magnetic fields of up to 300 mT. A low-energy beam available at PSI implants μ+ at variable depth in the London layer allowing for direct measurements of the London penetration depth from which other material parameters relevant for SRF applications, such as the lower critical field and the superheating field, can be calculated. Beta-detected nuclear magnetic resonance (β-NMR) is a technique similar to low-energy μSR using beams of low-energy β radioactive ions. With a recent upgrade, it is capable of detecting the penetration of parallel magnetic vortices, depth resolved with nanometer resolution at applied fields of up to 200 mT. In this paper, we review the impact and capabilities of these techniques for SRF research.

Depth-resolved Characterization of Meissner Screening Breakdown in Surface Treated Niobium

“…Non-destructive bulk measurements of the fields inside superconductors have been performed using techniques utilizing spin-polarized beams such as high-energy muons (so-called conventional muons with a nominal energy of 4 MeV) 12,27 and neutrons 26 . Depth-resolved and local measurements of the surface field in SRF samples have been performed using the low-energy muon spin rotation (LE-µSR) technique [28][29][30] . However, the LE-µSR technique is limited to low applied fields of ≤30 mT 31,32 -far less than the typical magnitude of B c1 or B sh of Nb.…”