Spectrophotometric method for the determination of uranium in urine

The effect of Y2O3 on the dynamics of oxidative dissolution of UO2

“…powder from Fluka, and the puriss potassium iodide powder for measuring the H 2 O 2 concentration came from KEBO lab. Both analytical methods have been described in detail [42][43][44][45]. All reagents were used as received.…”

H2 inhibition of radiation induced dissolution of spent nuclear fuel

“…The vessel was then irradiated in a 137 Cs gamma source Gammacell 1000 Elite from MDS Nordion with a dose rate of 0.15 Gy s À1 (determined using Fricke dosimetry [23]). After the desired irradiation time, the uranyl concentration in solution was measured using the Arsenazo III method with a S2000 spectrophotometer from WPA at a wavelength of 653 nm ( is 63 000 M À1 cm À1 ) described in [24,25]. Sample (1.5 mL) was mixed with 40 lL 0.03% Arsenazo III reagent and 65 lL 1 M HCl.…”

On the effects of fission product noble metal inclusions on the kinetics of radiation induced dissolution of spent nuclear fuel

“…The uranyl concentration was also measured by UV-vis spectroscopy at 653 nm with the Arsenazo III method [26,27]. and 650 lL 1 M HCl were mixed for that purpose.…”