Spectroelectrochemical sensing of reaction intermediates and products in an affordable fully 3D printed device

Šikula, Martin; Vaněčková, Eva; Hromadová, Magdaléna; Kolivoška, Viliam

doi:10.1016/j.aca.2023.341379

Analytica Chimica Acta

2023

DOI: 10.1016/j.aca.2023.341379

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Spectroelectrochemical sensing of reaction intermediates and products in an affordable fully 3D printed device

Martin Šikula,

Eva Vaněčková,

Magdaléna Hromadová

et al.

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Cited by 3 publications

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Multiscale characterisation of the electrical response of 3d printed carbon black polylactic acid

Robin,

Thomas,

Laurane

et al. 2023

J Mater Sci

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In this paper, the electrical response of a carbon black polylactic acid 3D printed polymer is characterised in detail by a combination of advanced experimental techniques at different scale lengths. The electrical properties as a function of the temperature become repeatable after the second heating cycle, exhibiting different trends as a function of the printing parameters. Joule heating and oven-heating techniques have been compared, showing the advantages of the Joule heating method to maintain electrical conductivity due to the lower thermal inertia. Small-Angle X-Ray Scattering has been employed to discern the underlying physics, showing the crucial role of crystallinity, filler dispersion and carbon black aggregates to form an effective segregated conductive network. This investigation provides guidelines to produce 3D-printed devices with a reliable electrical response and the governing equations to operate them with sufficient accuracy for engineering applications. Graphical abstract

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Multiscale characterisation of the electrical response of 3d printed carbon black polylactic acid

Robin,

Thomas,

Laurane

et al. 2023

J Mater Sci

View full text Add to dashboard Cite

show abstract

Pencil graphite electrodes for in-situ spectroelectrochemical sensing of reaction intermediates and products in organic solvents

Vaněčková,

Hrdlička,

Šebera

et al. 2024

Analytica Chimica Acta

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3D printed graphite-based electrode coupled with batch injection analysis: An affordable high-throughput strategy for atorvastatin determination

Faria

Nascimento

Villafuerte

et al. 2023

Talanta

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Spectroelectrochemical sensing of reaction intermediates and products in an affordable fully 3D printed device

Cited by 3 publications

References 81 publications

Multiscale characterisation of the electrical response of 3d printed carbon black polylactic acid

Multiscale characterisation of the electrical response of 3d printed carbon black polylactic acid

Pencil graphite electrodes for in-situ spectroelectrochemical sensing of reaction intermediates and products in organic solvents

3D printed graphite-based electrode coupled with batch injection analysis: An affordable high-throughput strategy for atorvastatin determination

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