Solvent effect on synthesis of indium tin oxide nano-powders by a solvothermal process

Lee, Jin-Seok; Choi, Seok Cheol

doi:10.1016/j.jeurceramsoc.2004.08.022

Cited by 88 publications

(32 citation statements)

References 29 publications

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“…This can enhance nucleation and grain growth [47,48]. Also, solvent viscosity determines the size and chemical properties [49]. PH can be a deciding factor for structural stability, composition, size and morphology control [50,51].…”

Section: Optical Electrical and Thermal Properties Of Ctsmentioning

confidence: 99%

Chemical synthesis of Cu 2 SnS 3 (CTS) nanoparticles: A status review

Lokhande

Gurav

et al. 2016

Journal of Alloys and Compounds

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Section: Optical Electrical and Thermal Properties Of Ctsmentioning

confidence: 99%

Chemical synthesis of Cu 2 SnS 3 (CTS) nanoparticles: A status review

Lokhande

Gurav

et al. 2016

Journal of Alloys and Compounds

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“…OH] improved the crystal growth rate compared to the nucleation rate and, in parallel, induced the formation of oxygen vacancies leading to more free electrons and higher conductivity [94]. The role of the viscosity of the solvent has also been underlined for the morphological control of rare earth oxide nanoparticles by solvothermal reaction [95].…”

Section: Role Of the Solvent In Materials Sciencementioning

confidence: 99%

Solvothermal and hydrothermal processes: the main physico-chemical factors involved and new trends

Demazeau¹

2011

Res Chem Intermed

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Hydro-and solvothermal processes play an important role in the different scientific domains involving either basic or applied research. During the last years, such processes have been strongly developed, in particular with the elaboration of nanocrystallites. This review article presents a brief history of their development, an analysis of the key factors governing such processes, and the recent trends.

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“…There are various processes for the preparation of ITO powders, such as co-precipitation [11], sol-gel [12], emulsion technique [13], hydrothermal and solvothermal process [14,15], microwave synthesis [16] and ultrasonic spray pyrolysis [17]. Compared with these reported methods, ultrasonic spray pyrolysis (USP) is convenient and simple for the preparation of such materials with controlled size and high purity [18][19][20].…”

Section: Introductionmentioning

confidence: 99%

Synthesis of indium tin oxide nano-polycrystalline powders by ultrasonic spray pyrolysis

et al. 2016

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Indium tin oxide (ITO) nano-polycrystalline powders were prepared by ultrasonic spray pyrolysis (USP) method using a precursor solution of indium and tin chlorides in a simple one-step process without any post-heat treatment, additives and other complex operations. The morphology and crystal structure of ITO powders were studied by thermogravimetric and differential thermal analysis (TG-DTA), X-ray diffraction (XRD), energy-dispersive spectrometer (EDS), scanning electron microscopy (SEM), laser particle size analyzer (LPSA), transmission electron microscope (TEM), high-resolution transmission electron microscopy (HRTEM) and selected area electron diffraction (SAED), respectively. The results indicate that pure cubic ITO solid solution could be obtained at and above the pyrolysis temperature of 600°C. Through adjusting the size of atomized precursor droplets, the particles with regular spherical shape and smooth surface are also obtained. The spherical particles have a narrow size distribution with a dominant diameter size in the range of 0.52-1.28 lm, and the average value is 1.01 lm. The clear lattice fringes in HRTEM image confirm a polycrystalline structure of ITO particles with the growth direction along (222) direction.

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Solvent effect on synthesis of indium tin oxide nano-powders by a solvothermal process

Cited by 88 publications

References 29 publications

Chemical synthesis of Cu 2 SnS 3 (CTS) nanoparticles: A status review

Chemical synthesis of Cu 2 SnS 3 (CTS) nanoparticles: A status review

Solvothermal and hydrothermal processes: the main physico-chemical factors involved and new trends

Synthesis of indium tin oxide nano-polycrystalline powders by ultrasonic spray pyrolysis

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