Sol-Gel Processing of Thin Films with Metal Salts

Nishio, K.; Tsuchiya, Toshio

doi:10.1007/978-3-319-32101-1_3

Cited by 4 publications

(5 citation statements)

References 49 publications

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“…The result confirms that the structures of the protein component of egg white in the form of amine and carboxyl groups are able to form a polypeptide bond through polymerization to produce ceramic nanoparticles at a low temperature [8,11,15]. These results is similar to the use of ethylene glycol by the Pechini method which is able to produce an agglomeration powder with crystal size 10 nm on yttria stabilized zirconia [8,16]. The typical SEM image of the MgPSZ sample heated at 700 0 C is shown in Figure 2.…”

Section: Resultssupporting

confidence: 72%

“…The majority crystal phase is tetragonal with the size of 8-26 nm, while the rest of the monoclinic crystals range from 18-42 nm. The result confirms that the structures of the protein component of egg white in the form of amine and carboxyl groups are able to form a polypeptide bond through polymerization to produce ceramic nanoparticles at a low temperature [8,11,15]. These results is similar to the use of ethylene glycol by the Pechini method which is able to produce an agglomeration powder with crystal size 10 nm on yttria stabilized zirconia [8,16].…”

Section: Resultssupporting

confidence: 66%

“…MgPSZ (Magnesia Partially Stabilized Zirconia) nanoparticle can be synthesized via sol-gel technique with a modified Pechini method using polymer precursors to produce a relatively low cost ceramics in low heat temperature with homogenous composition and high purity results [8]. The common polymer precursors are metal oxides, ethylene glycol, and citric acid.…”

Section: Introductionmentioning

confidence: 99%

“…The common polymer precursors are metal oxides, ethylene glycol, and citric acid. Ethylene glycol will facilitate the polymerization of metal oxide with citric acid became metal citrate [8]. However, this unique property is also possessed by the egg white or albumen.…”

Section: Introductionmentioning

confidence: 99%

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Synthesis and Characterization of MgPSZ-PMMA Composite by Sol-Gel Modification and Direct Foaming Technique Using Egg Whites

Takarini

Rudyawan²,

Hardiansyah³

et al. 2016

KEM

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This study prepared Magnesium-Partially Stabilized Zirconia (Mg-PSZ) filler synthesis and direct foaming technique using egg whites, and impregnated by PMMA. The results were evaluated systematically by X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Transmission Electron Microscope (TEM). XRD results denote that the powder sample of MgPSZ was successfully formed with various crystal size of tetragonal and monoclinic phase. SEM and TEM observations revealed that nanoparticles MgPSZ were in spherical and long rounded shapes. Furthermore, SEM observation revealed that the direct foaming method were also successful in the formation of porous structures which favourable for impregnation process by PMMA. The use of egg whites as a polymer precursor in both methods demonstrates that porous specimens contained nanosized, predominantly tetragonal, Mg-PSZ powders were successfully synthesized. This shall yield an interesting prospect towards cheap, reliable, and biocompatible product to resemble the modulus elasticity of dentin.

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Section: Resultssupporting

confidence: 72%

Section: Resultssupporting

confidence: 66%

Section: Introductionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

See 2 more Smart Citations

Synthesis and Characterization of MgPSZ-PMMA Composite by Sol-Gel Modification and Direct Foaming Technique Using Egg Whites

Takarini

Rudyawan²,

Hardiansyah³

et al. 2016

KEM

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“…In the sol–gel process, metal-based precursor salts transform into an oxide network via polymerization reactions. , These reactions occur by dissolving precursor salts into solvents forming solutions that can be spin-coated on substrates . This process accommodates essential advantages, such as low cost, composition tuning, and ambient processing conditions, thus allowing the synthesis of “tailor-made” materials. − Therefore, mastery of the sol–gel process requires accurate control over the various chemical reaction phases.…”

Section: Introductionmentioning

confidence: 99%

Physicochemical Analysis of Nanoscale Metal Oxide Thin Film Precursors via Infrared Spectroscopic Ellipsometry

Koutsiaki,

Koutsogeorgis,

Kalfagiannis

2023

J. Phys. Chem. C

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We present a nondestructive and highly sensitive experimental methodology for accurately controlling the chemical pathways of metal oxide formation in ultrathin films (∼10 nm) relevant for electronic devices, such as thin film transistors. Utilizing infrared spectroscopic ellipsometry (IRSE), we shed light on the individual sol–gel precursor conversion stages of In(NO3)3 and Zn(CH3COO)2 films into In2O3 and ZnO via a thermally induced reaction. Employing IR highly reflective substrates (TiN, Al, and Au), the intrinsic sensitivity of IRSE is enhanced; we present the chemical signatures of precursor byproducts, which are detected down to nanometer-scale thin films. We provide insights into the link between the chemical conversion, the substrate’s reflectivity, and IRSE sensitivity and propose a universal methodology for accurate physicochemical analysis of ultrathin films.

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Ultrasonically sprayed undoped and indium-doped titanium oxide thin films for methylene blue degradation: Effect of molarity and irradiation time

Gonzalez,

De La L. Olvera,

T.V.K.

et al. 2023

2023 20th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)

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Sol-Gel Processing of Thin Films with Metal Salts

Cited by 4 publications

References 49 publications

Synthesis and Characterization of MgPSZ-PMMA Composite by Sol-Gel Modification and Direct Foaming Technique Using Egg Whites

Synthesis and Characterization of MgPSZ-PMMA Composite by Sol-Gel Modification and Direct Foaming Technique Using Egg Whites

Physicochemical Analysis of Nanoscale Metal Oxide Thin Film Precursors via Infrared Spectroscopic Ellipsometry

Ultrasonically sprayed undoped and indium-doped titanium oxide thin films for methylene blue degradation: Effect of molarity and irradiation time

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