The aim of this study was to determine the individual variability in time to peak pH after the consumption of a 300mg . kg -1 dose of sodium bicarbonate (NaHCO 3 ). Seventeen active males volunteered to participate in the study (mean ± SD: age 21.38 ± 1.5y; mass 75.8 ± 5.8kg; height 176.8 ± 7.6cm). Participants reported to the laboratory where a resting capillary blood sample was taken aseptically from the fingertip. After this, 300 mg . kg -1 of NaHCO 3 in 400ml of water with 50ml of flavoured cordial was ingested.Participants then rested for 90 min during which repeated blood samples were procured at 10 minute intervals for 60 mins and then every 5 min until 90 min. Blood pH concentrations were measured using a blood gas analyser. Results suggested that time to peak pH (64.41±18.78 min) was highly variable with a range of 10-85 min and a coefficient of variation of 29.16%. A bi-modal distribution occurred, at 65 and 75 min. In conclusion, researchers and athletes, when using NaHCO 3 as an ergogenic aid, should determine, in advance their time to peak pH to best utilise the added buffering capacity this substance allows.