Smart regioselectivity towards mono 6-hydroxyl α-cyclodextrin amphiphilic derivatives

Cui, Yanli; Mao, Yangyi; Mao, Jianwei; Zhang, Yongmin

doi:10.1039/d0ra00299b

RSC Adv.

2020

DOI: 10.1039/d0ra00299b

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Smart regioselectivity towards mono 6-hydroxyl α-cyclodextrin amphiphilic derivatives

Yanli Cui

Yangyi Mao

Jianwei Mao

et al.

Abstract: A smart regioselective CD modification is described. For mono 6-hydroxyl and penta-alkyl coexistence on the primary face of α-CD, no additional catalysis or enzyme process are needed, just via adjustment of the ratio of alkali to alkylation agent.

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Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2019–2020

Harvey

2023

Mass Spectrometry Reviews

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This review is the tenth update of the original article published in 1999 on the application of matrix‐assisted laser desorption/ionization (MALDI) mass spectrometry to the analysis of carbohydrates and glycoconjugates and brings coverage of the literature to the end of 2020. Also included are papers that describe methods appropriate to analysis by MALDI, such as sample preparation techniques, even though the ionization method is not MALDI. The review is basically divided into three sections: (1) general aspects such as theory of the MALDI process, matrices, derivatization, MALDI imaging, fragmentation, quantification and the use of arrays. (2) Applications to various structural types such as oligo‐ and polysaccharides, glycoproteins, glycolipids, glycosides and biopharmaceuticals, and (3) other areas such as medicine, industrial processes and glycan synthesis where MALDI is extensively used. Much of the material relating to applications is presented in tabular form. The reported work shows increasing use of incorporation of new techniques such as ion mobility and the enormous impact that MALDI imaging is having. MALDI, although invented nearly 40 years ago is still an ideal technique for carbohydrate analysis and advancements in the technique and range of applications show little sign of diminishing.

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Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2019–2020

Harvey

2023

Mass Spectrometry Reviews

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Dexamethasone Sodium Phosphate Loaded Modified Cyclodextrin Based Nanoparticles: An Efficient Treatment for Rheumatoid Arthritis

Jadhav

Vavia

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Smart regioselectivity towards mono 6-hydroxyl α-cyclodextrin amphiphilic derivatives

Abstract: A smart regioselective CD modification is described. For mono 6-hydroxyl and penta-alkyl coexistence on the primary face of α-CD, no additional catalysis or enzyme process are needed, just via adjustment of the ratio of alkali to alkylation agent.

Cited by 2 publications

References 21 publications

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2019–2020

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2019–2020

Dexamethasone Sodium Phosphate Loaded Modified Cyclodextrin Based Nanoparticles: An Efficient Treatment for Rheumatoid Arthritis

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