The decay of K42 and its associated branching ratios have been investigated by several authors. The earlier works on the subject by SIEGBAHN et coll. and BLEULER & ZUNTI do not deal essentially with branching ratios. Later investigations by KAHN & LYON and EMERY & VEALL give respectively (20 ± 1) % and (17.8 ± 0.9) % of the beta disintegrations accompanied by a gamma quantum.K42 (half life 12.4 hours, 1.5 MeV y-ray) has proved to be a very useful isotope for human tracer studies. It is particularly important in investigations of electrolyte balance, and it is also used in determining body potassium by the potassium dilution method, as a tracer for studying potassium metabolism and in calibrating whole body counters. In all work of this type it would be valuable to have accurate knowledge of the branching ratio.In the present investigation anthracene and sodium iodide scintillation spectrometers were used as beta and gamma detectors respectively; both the composite beta spectrum and the spectrum of beta particles in coincidence with gamma quanta were determined. The pulse height distribution from the anthracene detector was recorded on a multichannel analyzer. In determining the pulse height distribution of beta particles in coincidence with gamma quanta, the multichannel analyzer was gated, e. g. only those pulses from the anthracene spectrometer were recorded which occurred simultaneously with the detection of a gamma quantum of energy 1.5 MeV by the sodium iodide spectrometer.