1983
DOI: 10.1016/0022-0248(83)90358-5
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Skull melter single crystal growth of magnetite (Fe3O4) - ulvospinel (Fe2TiO4) solid solution members

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Cited by 36 publications
(12 citation statements)
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“…AC electrical resistance measurements under external magnetic field were performed on PPMS apparatus on magnetite single crystal (triangle-like slice with exposed (1 0 0) type plane; TV = 123.7 K), skull melter grown from 99.99% pure Fe2O3 and annealed for stoichiometry [9].…”
Section: Methodsmentioning
confidence: 99%
“…AC electrical resistance measurements under external magnetic field were performed on PPMS apparatus on magnetite single crystal (triangle-like slice with exposed (1 0 0) type plane; TV = 123.7 K), skull melter grown from 99.99% pure Fe2O3 and annealed for stoichiometry [9].…”
Section: Methodsmentioning
confidence: 99%
“…22,23 The starting materials were 99.999% purity Fe 2 O 3 and 99.99 purity Al 2 O 3 . Single crystals ͑typically 15 mmϫ5 mmϫ5 mm͒ were isolated from the boules, analyzed for Al and Fe content by the electron microprobe technique, and checked by Laue back scattering, and x-ray powder diffraction.…”
Section: Methodsmentioning
confidence: 99%
“…The crystals were then subjected to subsolidus annealing under CO/CO 2 gas mixtures to establish the appropriate metal/oxygen ratio [22]. The actual composition and sample uniformity were checked using a microprobe electron [14][15][16] showing the characteristic break, differentiating first and second order Verwey transition.…”
Section: Sample Preparationmentioning
confidence: 99%