Studying the removal of rhodamine B (RB) dye by using zeolite 13X molecular sieves supported by Fe 2 O 3 nanoparticles (denoted as Fe 2 O 3 -13X) is the main objective of this study. Fe 2 O 3 -13X was synthesized and modified by the addition of sodium dodecyl sulfate (SDS). e prepared Fe 2 O 3 -13X was characterized by XRD, TEM, SEM, and zeta potential. e effects of the solution pH, SDS amount, contact time, initial dye concentration, and adsorbent dosage on the removal efficiency of RB were studied. A maximum removal efficiency of 99.3% was achieved. e adsorption equilibrium data of RB were fitted using the Freundlich model, yielding the maximum adsorption capacity of 89.3 mg/g. e findings revealed that the RB adsorption onto Fe 2 O 3 -13X modified with SDS (Fe2O3-13X-Ms) was described by a pseudo-second-order kinetic equation. e results reported in this paper indicate that a high RB removal percentage was attained by adding SDS to Fe 2 O 3 -13X.