Simultaneous determination of eight neonicotinoid insecticides, fipronil and its three transformation products in sediments by continuous solvent extraction coupled with liquid chromatography-tandem mass spectrometry

Wang, Zhiwei; Chen, Junhui; Zhan, Tianrong; He, Xiaolong; Wang, Baodong

doi:10.1016/j.ecoenv.2019.110002

Cited by 29 publications

(3 citation statements)

References 53 publications

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“…To date, numerous sample preparation methods for analysis have been developed. These include liquid–liquid extraction (Timofeeva et al 2017 ), liquid phase microextraction (Vichapong et al 2013 , 2019 ; Kachangoon et al 2020a , 2020b ), solid-phase extraction (Wang et al 2020b ; Zaidon et al 2019 ; Ghiasi et al 2020 ), QuEChERS (Paradis et al 2014 ; Tanner and Czerwenka 2011 ), and anion exchange-disposable pipette extraction (Song et al 2018 ). Following sample preparation, the next essential step is selecting the appropriate analytical method.…”

Section: Introductionmentioning

confidence: 99%

Reviewing neonicotinoid detection with electroanalytical methods

Barton,

Ullah,

Koszelska

et al. 2024

Environ Sci Pollut Res

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Neonicotinoids, as the fastest-growing class of insecticides, currently account for over 25% of the global pesticide market. Their effectiveness in controlling a wide range of pests that pose a threat to croplands, home yards/gardens, and golf course greens cannot be denied. However, the extensive use of neonicotinoids has resulted in significant declines in nontarget organisms such as pollinators, insects, and birds. Furthermore, the potential chronic, sublethal effects of these compounds on human health remain largely unknown. To address these pressing issues, it is crucial to explore and understand the capabilities of electrochemical sensors in detecting neonicotinoid residues. Surprisingly, despite the increasing importance of this topic, no comprehensive review article currently exists in the literature. Therefore, our proposed review aims to bridge this gap by providing a thorough analysis of the use of electrochemical methods for neonicotinoid determination. In this review article, we will delve into various aspects of electrochemical analysis, including the influence of electrode materials, employed techniques, and the different types of electrode mechanisms utilized. By synthesizing and analysing the existing research in this field, our review will offer valuable insights and guidance to researchers, scientists, and policymakers alike.

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Section: Introductionmentioning

confidence: 99%

Reviewing neonicotinoid detection with electroanalytical methods

Barton,

Ullah,

Koszelska

et al. 2024

Environ Sci Pollut Res

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“…Currently, thin-layer chromatography (TLC), 2,3 gas chromatography-mass spectrometry (GC-MS), 4,5 liquid chromatography-tandem mass spectrometry (LC-MS/MS), 6,7 and high-performance liquid chromatography (HPLC) 8,9 are the most common techniques used for detecting FP. However, complicated sample pretreatment, high cost, and reliance on well-trained personnel are some unfavourable characteristics of these detection techniques.…”

Section: Introductionmentioning

confidence: 99%

An electrochemical immunosensor based on a carboxylated multiwalled carbon nanotube-silver nanoparticle-chitosan functional layer for the detection of fipronil

Huang,

Hsiung,

2023

Nanoscale Adv.

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“…For this reason, the European Union has placed five neonicotinoid insecticides, including ACP, on the Watch List, i.e., the list of potentially hazardous pollutants. 7 Due to the high applicability of ACP as a pesticide despite its reported hazards, there are several methods reported for its determination recently, such as : surface-enhanced Raman spectroscopy (SERS), [8][9][10][11][12] liquid chromatography/mass spectroscopy (LC/MS), [13][14][15][16][17] ultra-high performance liquid chromatography (U-HPLC), [18][19][20] (HPLC), [21][22][23][24][25] spectrophotometry, [26][27][28] and fluorometry. [29][30][31][32][33] MIP based method fabricated over silica-carbon dots by sol-gel polymerization was used for fluorescent detection of ACP.…”

mentioning

confidence: 99%

Application of Molecularly Imprinted Electrochemical Sensor for Selective Non-Labelled Detection of Acetamiprid Insecticide in Fruits

Harery¹,

Ghani²,

Nashar³

2023

J. Electrochem. Soc.

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Acetamiprid (ACP) is a systemic insecticide widely used as a replacement for organophosphorus compounds to control sucking-type insects on leafy vegetables, fruits, and tea trees. In this work, bulk polymerized molecularly imprinted polymer was developed using ACP as template, 4-Vinyl pyridine as monomer and ethylene glycol dimethyl acrylate (EGDMA) as cross-linker in the presence of acetone as porogen. After evaluation of five polymeric ratios according to their equilibrium rebinding assay, the MIP comprising 1:3:50 (template: monomer: cross-linker) was found to show the best binding capacity, and thus was chosen as a template recognition for carbon paste electrode in cooperation with multiwalled carbon nanotubes as a signal enhancer. The developed electrode was morphologically and electrochemically characterized and was found to show a linear response for differential pulse voltammetry of 1 × 10-12 – 5 × 10-6 M equivalent to 0.222 – 111.3 ×104 ng/L with limits of detection and quantification of 7.35 × 10-3 and 0.022 ng/L, respectively. The electrode was efficiently applied for ACP detection in its pure solutions, commercial insecticide and spiked apple, tomato, and watermelon samples with recoveries from 95.55 -101.66% indicating its efficiency for application in regulatory units for hazardous food contaminants.

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Simultaneous determination of eight neonicotinoid insecticides, fipronil and its three transformation products in sediments by continuous solvent extraction coupled with liquid chromatography-tandem mass spectrometry

Cited by 29 publications

References 53 publications

Reviewing neonicotinoid detection with electroanalytical methods

Reviewing neonicotinoid detection with electroanalytical methods

An electrochemical immunosensor based on a carboxylated multiwalled carbon nanotube-silver nanoparticle-chitosan functional layer for the detection of fipronil

Application of Molecularly Imprinted Electrochemical Sensor for Selective Non-Labelled Detection of Acetamiprid Insecticide in Fruits

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