Highly resolved time series data are useful to accurately identify the timing, rate, and magnitude of solute transport in streams during hydrologically dynamic periods such as snowmelt. We used in situ optical sensors for nitrate (NO 3 -) and chromophoric dissolved organic matter fluorescence (FDOM) to measure surface water concentrations at 30 min intervals over the snowmelt period (March 21-May 13, 2009) at a 40.5 hectare forested watershed at Sleepers River, Vermont. We also collected discrete samples for laboratory absorbance and fluorescence as well as d 18 O-NO 3 -isotopes to help interpret the drivers of variable NO 3 -and FDOM concentrations measured in situ. In situ data revealed seasonal, event and diurnal patterns associated with hydrological and biogeochemical processes regulating stream NO 3 -and FDOM concentrations. An observed decrease in NO 3 -concentrations after peak snowmelt runoff and muted response to spring rainfall was consistent with the flushing of a limited supply of NO 3 -(mainly from nitrification) from source areas in surficial soils. Stream FDOM concentrations were coupled with flow throughout the study period, suggesting a strong hydrologic control on DOM concentrations in the stream. However, higher FDOM concentrations per unit streamflow after snowmelt likely reflected a greater hydraulic connectivity of the stream to leachable DOM sources in upland soils. We also observed diurnal NO 3 -variability of 1-2 lmol l -1 after snowpack ablation, presumably due to in-stream uptake prior to leafout. A comparison of NO 3 -and dissolved organic carbon yields (DOC, measured by FDOM proxy) calculated from weekly discrete samples and in situ data sub-sampled daily resulted in small to moderate differences over the entire study period (-4 to 1% for NO 3 -and -3 to -14% for DOC), but resulted in much larger differences for daily yields (-66 to ?27% for NO 3 -and -88 to ?47% for DOC, respectively). Despite challenges inherent in in situ sensor deployments in harsh seasonal conditions, these data provide important insights into processes controlling NO 3 -and FDOM in streams, and will be Electronic supplementary material The online version of this article (