The solution of 2-furaldehyde and L-lysine was heated at pH = 5.6, and the brown reaction mixture was separated into chloroform-soluble and chloroform-insoluble fractions. The chloroform extract was subfractionated by subsequent extractions with water, methanol, and chloroform. The three fractions widely differed in their sensory profiles, nevertheless, they mainly contained baked, spicy, oily, and nutty odour notes. The flavour resembled coffee extract or chicory. The chloroform-insoluble fraction was subfractionated by gel chromatography into seven subfractions with less intensive odour than that of chloroform-soluble fractions. Each subfraction possessed a different, characteristic odour, the odour profiles consisting of baked, meaty, sulphurous, rancid, and foul notes. The determination of odour profiles of flavour fractions was found a sensitive and accurate procedure for the detection and evaluation of minor changes of odour.