Sensitive detection of iron (II) sulfate with a novel reagent using spectrophotometry

Özkök, Funda; Şahin, Yeşim Müge; Atalay, Vildan Enisoğlu; Asgarova, Kamala; Onul, Nihal; Çatal, Tunç

doi:10.1016/j.saa.2020.118631

Cited by 4 publications

(2 citation statements)

References 60 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…In advance, different rations of the compounds could be used to enhance the sensitivity of the reaction with Catal's reagent. Catal's reagent can be used for spectrophotometric and colorimetric detection of iron (II) sulfate [4] .…”

Section: Experimental Design Materials and Methodsmentioning

confidence: 99%

Dataset on Catal's reagent: Sensitive detection of iron (II) sulfate using spectrophotometry

Özkök

Şahin

Atalay³

et al. 2020

Data in Brief

Self Cite

View full text Add to dashboard Cite

Catal's reagent is characterized by spectroscopic methods such as fourier-transform infrared spectroscopy (FT-IR), nuclear magnetic resonance (NMR) spectroscopy, mass spectrometry (MS), ultraviolet (UV)–visible spectrophotometry. Effects of different solvents such as methanol and ethanol on absorption spectrum of 1-(Dodecylthio)anthracene-9,10-dione (3) were present. Detection range of iron (II) sulfate using Catal's reagent was analyzed. Synthesis of 1-(Dodecylthio)anthracene-9,10-dione ( 3 ) was explained, and absorbances of various concentrations of iron (II) sulfate (0- 10 mg mL −1 ) were measured. The possible detection mechanism was also explained. The dataset is useful to improve the detection of iron (II) sulfate in various application fields such as environmental, agricultural, sensor, food, textile and cement industries. The study refers to: F. Ozkok, Y.M. Sahin, V. Enisoglu-Atalay, K. Asgarova, N. Onul, T. Catal, Sensitive Detection of Iron (II) Sulfate with a Novel Reagent using Spectrophotometry, Spectchim. Acta. A, 240 (2020), 118631. https://doi.org/10.1016/j.saa.2020.118631 .

show abstract

Section: Experimental Design Materials and Methodsmentioning

confidence: 99%

Dataset on Catal's reagent: Sensitive detection of iron (II) sulfate using spectrophotometry

Özkök

Şahin

Atalay³

et al. 2020

Data in Brief

Self Cite

View full text Add to dashboard Cite

show abstract

“…In this study, compounds 3 and 5 were synthesized in a previous study (1). Various bioactive amino-and thioanthraquinone analogues were synthesized in our previous studies (45)(46). In this work, enzyme, in silico and in vitro study of these compounds were performed.…”

Section: Synthesismentioning

confidence: 99%

Evaluation of Acetyl- and Butyrylcholinesterase Enzyme Inhibitory Activities and Cytotoxic Activities of Anthraquinone Derivatives

OZKOK

Boğa

TUNEG

et al. 2022

Journal of the Turkish Chemical Society Section A: Chemistry

Self Cite

View full text Add to dashboard Cite

In this study, the enzyme activity of anthraquinone compounds which were synthesized beforehand by our research group was investigated. Molecular docking studies were performed for compounds 1-(4-aminophenylthio)anthracene-9,10-dione (3) and 1-(4-chlorophenylthio)anthracene-9,10-dione (5). Compound 3 was synthesized from the reaction of 1-chloroanthraquinone (1) and 4aminothiophenol (2). Compound 5 was synthesized (1) from the reaction of 1-chloroanthraquinone (1) and 4-chlorothiophenol (4). Anthraquinone analogs (3, 5) were synthesized with a new reaction method made by our research group (2). Inhibitory effects of compounds 3 and 5 were investigated against acetylcholinesterase (AChE) and butyrylcholinesterase (BuChE) enzymes which are related to Alzheimer's Disease (AD). Compounds 3 and 5 exhibited strong anti-acetyl-and butyryl-cholinesterase inhibition activities than galanthamine used as standard compound (92.11±1.08 and 80.95±1.77 %, respectively). The EHOMO-ELUMO values, molecular descriptors, and the calculated UV-Vis spectra of anthraquinone derivatives were computed by B3LYP/6-31+G(d,p) levels in the CHCl3 phase. Based on the fluorescence property of the anthraquinone skeleton, the fluorescence activity of the bioactive anthraquinone analogue (5) was investigated. MTT test was performed to determine the cytotoxic effects of thioanthraquinone molecules 3 and 5. In MTT analyses, 3 compounds showed the highest effect against Ishikawa cells at a dose of 10 µg/mL, while compound 5 showed the highest effect at a dose of 50 µg/mL. The cell viability for compound 3 was 84.18% for 10 µg/mL and the cell viability for compound 5 was 75.02% for 50 µg/mL.

show abstract

Inorganic phosphate regulated high luminescence NaYF4:Yb3+, Er3+ as an iron ion fluorescent nanoprobe

Song

Zhu

Wang

et al. 2023

Spectrochimica Acta Part A: Molecular and Biomolecular Spectros

View full text Add to dashboard Cite

Sensitive detection of iron (II) sulfate with a novel reagent using spectrophotometry

Cited by 4 publications

References 60 publications

Dataset on Catal's reagent: Sensitive detection of iron (II) sulfate using spectrophotometry

Dataset on Catal's reagent: Sensitive detection of iron (II) sulfate using spectrophotometry

Evaluation of Acetyl- and Butyrylcholinesterase Enzyme Inhibitory Activities and Cytotoxic Activities of Anthraquinone Derivatives

Inorganic phosphate regulated high luminescence NaYF4:Yb3+, Er3+ as an iron ion fluorescent nanoprobe

Contact Info

Product

Resources

About