“…Without ultra-sonication, there are fewer chances for electrostatic interactions and nanohybrid formation since there is not enough kinetic energy. 31,32 Fabrication of the working electrode, and electrochemical studies For the typical fabrication of the working interface, 1 mg of Fe 2 O 3 , Fe 2 O 3 @Ni, and porphyrin + Fe 2 O 3 @Ni (1 : 1) was added to 1 mL of distilled water, ethanol and ethanol : water, respectively. These mixtures were then ultra-sonicated for 15 minutes to obtain homogeneous dispersions.…”