In situ three terminal electron field emission characterization of an isolated multiwalled carbon nanotube has been performed, where both anode and gate electrodes are attached to high precision piezodrivers. All measurements are performed in a scanning electron microscope allowing accurate knowledge of the local environment of the nanotube to be obtained. It is shown that the presence of the grounded gate electrode screens the applied field by approximately 32%. This technique in positioning the gate and anode electrodes allows for an estimate of the gate transparency factor and demonstrates characterization of individual carbon nanotubes without the need for fabrication of arrays of emitters. © 2006 American Institute of Physics. ͓DOI: 10.1063/1.2335604͔Since the identification of carbon nanotubes ͑CNTs͒, 1 there has been sustained research into numerous potential applications of CNTs, in particular, for applications in field emission. 2,3 The high aspect ratio of a CNT results in a high local electric field for a given macroscopic field. As a result their use as electron sources for field emission based flat panel displays has been greatly explored, with the emergence of prototype displays. 4 While extensive two terminal field emission measurements have been performed, 2-6 considerably fewer three terminal studies 7-10 have been undertaken and those that have been performed have often been from arrays of nanotubes. In this letter we demonstrate a method of examining the gated field emission properties of an individual CNT and a method for establishing the gate transparency factor and the shielding of the emitter due to the presence of the gate itself. By performing the measurements in a scanning electron microscope ͑SEM͒ with electrodes attached to manipulators, we are able to investigate individual emitters, with a degree of freedom to move the electrodes in real time. Our approach opens the possibility of an effective method for testing the performance of a range of emitter structures prior to fabricating a prototype device, where the characteristics of an ensemble of emitters are measured. In addition, an ability to test single emitters may lead the way to enhance the emission uniformity from CNTs and increase the fraction of nanotubes that are actively emitting.Multiwalled carbon nanotubes were synthesized by a plasma arc discharge system between two graphite electrodes. The subsequent carbon deposit was purified by microfiltering and oxidization at 500°C to remove any amorphous carbon and carbon particulates, leaving purified CNTs. The CNTs were mixed into a polymer solution of polystyrene, which was dissolved in toluene. An ultrasonic treatment was used to improve the dispersion of the CNTs within the polymer. Vacuum casting methods were then used and the as-cast films were hot pressed to remove any residual solvent. To expose a single CNT the sample was mechanically broken and the broken edge studied in a Cambridge Instruments Stereoscan 250 III scanning electron microscope. A single CNT with a height ...