Selective solid-phase extraction using molecularly imprinted polymers for analysis of venlafaxine, O-desmethylvenlafaxine, and N-desmethylvenlafaxine in plasma samples by liquid chromatography–tandem mass spectrometry

Miranda, Luís Felippe Cabral; Domingues, Diego Soares; Queiroz, Maria Eugênia Costa

doi:10.1016/j.chroma.2016.06.024

Cited by 36 publications

(7 citation statements)

References 31 publications

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“…When reviewing the literature, one frequently comes across 4.65 as the value reported for pKa of MAA, which forms the main body of the polymer. This means that COOH functional groups are converted into COOH 2+ in acidic environments (>4.65) and gain a positive partial charge (Miranda et al, ). While CLO is also positive in acidic environments, repulsive positive charges interfere with the interaction between the CLO functional groups and the carbonyl groups of MAA.…”

Section: Resultsmentioning

confidence: 99%

Synthesis and characterisation of a selective adsorbent based on the molecularly imprinted polymer for the removal of cloxacillin antibiotic residue from milk

Jafari

Dehghani

Nasirizadeh

et al. 2019

Int J of Dairy Tech

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In recent decades, environmental pollution has been a subject of growing concern. This is partly due to the overuse of antibiotics, the consequent drug resistance and the discharge of drugs into the environment. The aim of this study was to synthesise molecularly imprinted polymer (MIP) particles via a noncovalent procedure for the removal of cloxacillin from milk. Accordingly, the effects of operational parameters such as pH, contact time and MIP dosage were studied. The performance of MIP particles in removing cloxacillin from livestock milk samples proved that these adsorbents can effectively help to reduce drug contamination from dairy sources.

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Section: Resultsmentioning

confidence: 99%

Synthesis and characterisation of a selective adsorbent based on the molecularly imprinted polymer for the removal of cloxacillin antibiotic residue from milk

Jafari

Dehghani

Nasirizadeh

et al. 2019

Int J of Dairy Tech

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“…VEN overdose, on the other hand, can induce symptoms such as hypertension, serotonin toxicity, seizures, or cardiac conduction disorders, necessitating therapeutic monitoring of this medication. VEN undergoes substantial metabolization to one main active O-desmethyl metabolite and two minor metabolites, which are subsequently combined to create O-desmethylvenlafaxine (ODV), N10 desmethylvenlafaxine (NDV), and N,O -didesmethylvenlafaxine (NDV) (Miranda et al 2016 ). Analysis of VEN, ODV, and NDV in plasma samples by molecularly imprinted solid phase extraction coupled via UHPLC-MS/MS (MISPE/UHPLC-MS/MS) is performed by Miranda et al ( 2016 ).…”

Section: Mip In Bioanalysismentioning

confidence: 99%

Recent molecularly imprinted polymers applications in bioanalysis

Suzaei¹,

Daryanavard

Abdel-Rehim

et al. 2022

Chem. Pap.

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Molecular imprinted polymers (MIPs) as extraordinary compounds with unique features have presented a wide range of applications and benefits to researchers. In particular when used as a sorbent in sample preparation methods for the analysis of biological samples and complex matrices. Its application in the extraction of medicinal species has attracted much attention and a growing interest. This review focus on articles and research that deals with the application of MIPs in the analysis of components such as biomarkers, drugs, hormones, blockers and inhibitors, especially in biological matrices. The studies based on MIP applications in bioanalysis and the deployment of MIPs in high-throughput settings and optimization of extraction methods are presented. A review of more than 200 articles and research works clearly shows that the superiority of MIP techniques lies in high accuracy, reproducibility, sensitivity, speed and cost effectiveness which make them suitable for clinical usage. Furthermore, this review present MIP-based extraction techniques and MIP-biosensors which are categorized on their classes based on common properties of target components. Extraction methods, studied sample matrices, target analytes, analytical techniques and their results for each study are described. Investigations indicate satisfactory results using MIP-based bioanalysis. According to the increasing number of studies on method development over the last decade, the use of MIPs in bioanalysis is growing and will further expand the scope of MIP applications for less studied samples and analytes.

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“…An interesting SPE technique for the preparation of human plasma samples containing venlafaxine and desvenlafaxine was described by Miranda, Domingues, and Queiroz (). A novel miniaturized molecularly imprinted polymer (MIP) was synthesized to act as a selective SPE material.…”

Section: Techniquesmentioning

confidence: 99%

“…An interesting SPE technique for the preparation of human plasma samples containing venlafaxine and desvenlafaxine was described by Miranda, Domingues, and Queiroz (2016). A novel minia- In the method developed by Ghorbani, Chamsaz, and Rounaghi (2016), human urine samples of venlafaxine and desvenlafaxine were extracted by SPME and then quantitated using HPLC-PDA.…”

Section: Venlafaxine and Desvenlafaxine (O-desmethyl Venlafaxine)mentioning

confidence: 99%

Recent advances in liquid chromatographic methods for the determination of selective serotonin reuptake inhibitors and serotonin norepinephrine reuptake inhibitors

Jia

Bartlett

2020

Biomedical Chromatography

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Depression is now the second largest public health burden throughout the world. Selective serotonin reuptake inhibitors (SSRIs) and serotonin norepinephrine reuptake inhibitors (SNRIs) have replaced older antidepressants to become first‐line medications to treat this disease with increased remission rates and markedly decreased incidence of severe adverse events. Traditional and modern bioanalytical strategies for SSRI and SNRI determination are being continuously improved. There has also been a recent increase in the use of unconventional sample preparation methods. This review critically evaluates the development of SSRI and SNRI liquid chromatographic analytical methods published between 2014 and mid‐2019, with special attention to novel sample preparation methods.

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Selective solid-phase extraction using molecularly imprinted polymers for analysis of venlafaxine, O-desmethylvenlafaxine, and N-desmethylvenlafaxine in plasma samples by liquid chromatography–tandem mass spectrometry

Cited by 36 publications

References 31 publications

Synthesis and characterisation of a selective adsorbent based on the molecularly imprinted polymer for the removal of cloxacillin antibiotic residue from milk

Synthesis and characterisation of a selective adsorbent based on the molecularly imprinted polymer for the removal of cloxacillin antibiotic residue from milk

Recent molecularly imprinted polymers applications in bioanalysis

Recent advances in liquid chromatographic methods for the determination of selective serotonin reuptake inhibitors and serotonin norepinephrine reuptake inhibitors

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