2013
DOI: 10.1007/s00128-013-1162-9
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Selective Pressurized Liquid Extraction Technique Capable of Analyzing Dioxins, Furans, and PCBs in Clams and Crab Tissue

Abstract: A selective pressurized liquid extraction technique (SPLE) was developed for the analysis of polychlorodibenzo-p-dioxins, polychlorodibenzofurans (PCDD/Fs) and dioxin-like polychlorobiphenyls (dl-PCBs) in clam and crab tissue. The SPLE incorporated multiple cleanup adsorbents (alumina, florisil, silica gel, celite, and carbopack) within the extraction cell. Tissue extracts were analyzed by high resolution gas chromatography coupled with electron capture negative ionization mass spectrometry. Mean recovery (n =… Show more

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Cited by 8 publications
(3 citation statements)
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“…Solvent extraction was advised for dust and soil samples that have big particles, such as pebbles and twigs [36].…”
Section: The Most Common Methods For Analysis and Detectionmentioning
confidence: 99%
“…Solvent extraction was advised for dust and soil samples that have big particles, such as pebbles and twigs [36].…”
Section: The Most Common Methods For Analysis and Detectionmentioning
confidence: 99%
“…Because of all these steps, the analysis is particularly long and expensive. The development of S-PLE methods allowed the analysis of these contaminants in food matrices involving fat removal directly in the extraction cell (in the presence of clean-up sorbent) in order to obtain extracts suitable for direct GC analysis [16][17][18]20] or further purification steps (SPE) [22,23].…”
Section: Edcsmentioning
confidence: 99%
“…Carbopack, dispersed in celite, is typically used to fractionate planar compounds (PCDD/Fs) from the non-planar compounds (PCBs), known to interfere between them [57].…”
Section: [Insert Figure 4]mentioning
confidence: 99%