In the last decade a major progress has been achieved in the synthesis and functionalization of nanoscale particles, but the handling of such material systems like separation or classification has been neglected. With tubular centrifuges, even nanoscale particles can be separated from a suspension at reasonable throughputs due to very high g values. This is a great advantage compared to membrane techniques (low throughput) and filtering, disc stack and decanter centrifuges (lower g values). An analysis of the discharged solids in dependence on time and verification of sediment build-up with a magnetic resonance spectrometer (MRI) provide a comprehensive understanding of the sedimentation process in a tubular bowl centrifuge. MRI allows a noninvasive, direct view into the filled centrifuge rotor; this data is compared with theoretical results.