A near-surface seismic refraction survey was conducted at a new mining area located in southeast Cairo, Egypt, to explore the subsurface clay layer for future economic use in mining and cement industry. The purpose of the survey has been to provide geological and geophysical information because no borehole was existent in the area under investigation. The aim of study had been to explain the main characteristics of the subsurface layers. For this purpose, a new technique has been used to acquire and process the data. This technique provides critical information to determine the depth of the subsurface layers, as well as morphology, stratigraphy, and potential locations of the clay layer for future economic use. The thickness and general shape of the clay layer in the whole area were determined and are illustrated in maps.