2013
DOI: 10.1039/c2cc37241j
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Schischkiniin support studies: synthetic access to 1,1′-bisindoles

Abstract: The first general synthetic approach to 1,1'-bisindoles is described. Two simultaneous, ambient temperature Mori-Ban reactions were used to effect bisindolization of several diallylated hydrazobenzenes with minimal cleavage of the N-N bond.

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Cited by 25 publications
(21 citation statements)
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“…TXM analysis has utilized the beamline 01B1 facility of the National Synchrotron Radiation Research Center (NSRRC) in Taiwan, and results from a detailed study of the SnO electrode analyzed during the first two lithiation-delithiation cycles have been published . Within the past few years, the importance of high-resolution in situ X-ray microscopy for studying high-capacity secondary batteries has become apparent Chao et al, 2010;Wang, Chen-Wiegart et al, 2013). In situ TXM research in combination with XANES on battery materials was carried out to achieve the necessary characterization of the phase and chemical states as well as the morphology evolution at nanometer resolution .…”
Section: Transmission X-ray Microscopymentioning
confidence: 99%
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“…TXM analysis has utilized the beamline 01B1 facility of the National Synchrotron Radiation Research Center (NSRRC) in Taiwan, and results from a detailed study of the SnO electrode analyzed during the first two lithiation-delithiation cycles have been published . Within the past few years, the importance of high-resolution in situ X-ray microscopy for studying high-capacity secondary batteries has become apparent Chao et al, 2010;Wang, Chen-Wiegart et al, 2013). In situ TXM research in combination with XANES on battery materials was carried out to achieve the necessary characterization of the phase and chemical states as well as the morphology evolution at nanometer resolution .…”
Section: Transmission X-ray Microscopymentioning
confidence: 99%
“…Additionally, TXM is the synchrotronbased full-field imaging method that acquires a complete image on a direct imaging base with the highest resolution and is the best suited for morphological studies on dynamic events and microtomography (Kaulich et al, 2009). It can also perform two-dimensional imaging on several materials such as fuel cells and battery electrodes and has received increasing interest for applications in different fields of study (Li et al, 2016;Singh et al, 2012;Wang, Chen-Wiegart et al, 2013).…”
Section: Introduction To In Situ Synchrotron Techniquesmentioning
confidence: 99%
“…As seen from the work of Nishida, the conjugated double bond (vinylogous carbamate) can isomerize as necessary to set up the Heck cyclization (equation 5) [15]. A Mori-Ban indole synthesis has featured prominently in the syntheses of (±)-aspidophytine [16], stephacidin A [17], 1,1′-bisindoles [18], a potent EP 3 receptor antagonist (DG-041) [19], kinesin spindle protein inhibitors [20], hepatitis C protein inhibitors [21], and S1P 1 agonists [22].…”
Section: The Mori-ban Indole Synthesis Is a Pd-catalyzed Cyclization mentioning
confidence: 99%
“…9,10 This new methodology relied on several diallylated hydrazobenzenes undergoing two simultaneous Mori-Ban cyclizations to construct both heterocycles in a single step with minimal N-N bond cleavage. J. Sperry Developing a general synthetic approach to 1,1′-bisindoles (Scheme 1).…”
Section: Synform What Is Your Most Important Scientific Achievement Tmentioning
confidence: 99%