1985
DOI: 10.1016/s0020-1693(00)86563-9
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[Ru2(μ-4-F-C6H4CO2)2(CO)5H2O]: Molecular structure and catalytic activity

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Cited by 6 publications
(2 citation statements)
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“…Some starting hexacarbonyl (0.010 g) and some [Os,(MeC0,),(CO),(PPh3)2] (0.015 g) were also obtained. (0.100 g) as yellow crystals (0.060 g, 57%) (Found: C, 26.2; H, 2.25; P, 3 (0.1 10 g) in acetonitrile (20 cm3) was heated under reflux for 30 min. Evaporation of the solvent gave the product as somewhat air-sensitive pale yellow plates (0.101 g, 88%) (Found: C, 21.2; H, 1.8; N, 3.9.…”
Section: Synthesis Of [Os(meco)(co)(pph)]-amentioning
confidence: 99%
“…Some starting hexacarbonyl (0.010 g) and some [Os,(MeC0,),(CO),(PPh3)2] (0.015 g) were also obtained. (0.100 g) as yellow crystals (0.060 g, 57%) (Found: C, 26.2; H, 2.25; P, 3 (0.1 10 g) in acetonitrile (20 cm3) was heated under reflux for 30 min. Evaporation of the solvent gave the product as somewhat air-sensitive pale yellow plates (0.101 g, 88%) (Found: C, 21.2; H, 1.8; N, 3.9.…”
Section: Synthesis Of [Os(meco)(co)(pph)]-amentioning
confidence: 99%
“…For O donor ligands in the terminal positions the crystal structures of only two aqua complexes were described in the literature. In this context the molecular structure of [Ru 2 (m-O 2 CC 6 H 4 eF) 2 (CO) 5 (OH 2 )] was reported [14]. The distance RueO(aqua) in the latter compound was found to be 2.299(6) Å and is therefore in a good accordance with the corresponding bond lengths found for 2, Ru1eO7, 2.2906 (13), and Ru2eO8, 2.2802(17), respectively.…”
Section: Molecular Structures Of Compounds 2 Andmentioning
confidence: 99%