[Ru2(μ-4-F-C6H4CO2)2(CO)5H2O]: Molecular structure and catalytic activity

Rotem, Michal; Goldberg, Israel; Shvo, Youval

doi:10.1016/s0020-1693(00)86563-9

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Synthesis Of [Os(meco)(co)(pph)]-a1

Molecular Structures Of Compounds 2 And1

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1986

2014

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Cited by 6 publications

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“…Some starting hexacarbonyl (0.010 g) and some [Os,(MeC0,),(CO),(PPh3)2] (0.015 g) were also obtained. (0.100 g) as yellow crystals (0.060 g, 57%) (Found: C, 26.2; H, 2.25; P, 3 (0.1 10 g) in acetonitrile (20 cm3) was heated under reflux for 30 min. Evaporation of the solvent gave the product as somewhat air-sensitive pale yellow plates (0.101 g, 88%) (Found: C, 21.2; H, 1.8; N, 3.9.…”

Section: Synthesis Of [Os(meco)(co)(pph)]-amentioning

confidence: 99%

Substitution reactions of the osmium(I) dinuclear compound [Os2(MeCO2)2(CO)6]. X-Ray crystal structure of [N(PPh3)2][Os2(MeCO2)2Cl(CO)5]

Deeming¹,

Randle²,

Hursthouse³

et al. 1987

J. Chem. Soc., Dalton Trans.

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Section: Synthesis Of [Os(meco)(co)(pph)]-amentioning

confidence: 99%

Substitution reactions of the osmium(I) dinuclear compound [Os2(MeCO2)2(CO)6]. X-Ray crystal structure of [N(PPh3)2][Os2(MeCO2)2Cl(CO)5]

Deeming¹,

Randle²,

Hursthouse³

et al. 1987

J. Chem. Soc., Dalton Trans.

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“…For O donor ligands in the terminal positions the crystal structures of only two aqua complexes were described in the literature. In this context the molecular structure of [Ru 2 (m-O 2 CC 6 H 4 eF) 2 (CO) 5 (OH 2 )] was reported [14]. The distance RueO(aqua) in the latter compound was found to be 2.299(6) Å and is therefore in a good accordance with the corresponding bond lengths found for 2, Ru1eO7, 2.2906 (13), and Ru2eO8, 2.2802(17), respectively.…”

Section: Molecular Structures Of Compounds 2 Andmentioning

confidence: 99%