A number of pedagogical methods have been used to enhance learning in the laboratory setting. These include problem-based learning (e.g., 1-5), cooperative learning (e.g.,(6, 7)), service learning (e.g., [8][9][10][11], and role-playing (e.g., 12-16). These methods reinforce course content and also enhance communication, critical thinking, and problemsolving skills. Historically, analytical chemistry laboratories have focused on students obtaining the "right answer". In our experience teaching both quantitative analysis and instrumental analysis laboratory courses, we have found that students were more concerned with obtaining the right answer than critically thinking about the significance of the number. In an effort to help students develop critical-thinking skills in the context of analytical chemistry, we have instituted a major pedagogical change in the second-year instrumental analysis laboratory. This change first occurred in the fall 2005 semester and we have just completed the fourth year of this implementation. We have chosen to explore a multifaceted approach that combines many of the favorable components of the aforementioned learning techniques.Our goals in organizing the laboratory include (i) group or cooperative learning; (ii) real-world sample analysis; (iii) roleplaying from multiple points of the employment spectrum; (iv) exposure to multiple methods of scientific presentation including written, oral, and poster formats; and (v) development of a teaching method that could be easily adopted from standard analytical laboratories without significant laboratory development. Additionally, we have made it our strict policy that instructors or teaching assistants never tell the students the "right" answer. It is our view that in their future careers as scientists they will need to rely on their own laboratory skills and data to judge the "rightness" of an answer; there will never be an instance when they are presented with the right answer.
Course DesignThe instrumental analysis laboratory course is offered to chemistry majors and is typically taken by second-year students, although upper-level students are often also enrolled. The laboratory consists of a four-hour laboratory and a one-hour recitation each week. A three-hour instrumental analysis classroom lecture course is a corequisite. Our newly designed laboratory curriculum consists of four three-week experiments, each dealing with a unique application of instrumental analysis exposing the students to approximately nine analytical instruments. We have designed laboratory-based, role-playing scenarios focused on more routine topics of pharmaceutical, forensic, environmental, and food chemistry, as well as specialized topics including gemology and art conservation that are rotated each semester.