“… 48,55,56 Copper peaks were present at 2 θ = 43.7°, 50.8°, and 74.4° due to the copper substrate, and the very broad peaks at 44.7° were ascribed to the (111) of amorphous Ni–P alloy. 57 The Au (111), Au (220), and Au (300) diffraction peaks were detected at 38.6°, 65.1°, and 78.0°, respectively, and the Au (111) was the preferred orientation. The XRD patterns of the gold peaks of five kinds of coatings were similar, indicating that the addition of NaH 2 PO 2 did not affect the crystal structure of gold regardless of the NaH 2 PO 2 concentration.…”