2024
DOI: 10.21577/0103-5053.20230095
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Revisiting the Synthesis of Gibbsite, a Precursor for Li/Al LDH Synthesis and Its Use as a Support for Porphyrin Immobilization

Gabriela Bosa,
Caroline Silva,
Bianca Brito
et al.

Abstract: In this work, some of the synthesis methods already reported for aluminum(III) hydroxide polymorphs with layered structure like gibbsite are revisited. Gibbsite was synthesized with high purity and yield by a simple route developed from modifications of a heating method proposed in the literature, making it possible to prepare gibbsite in regular glassware, avoiding the use of hydrothermal reactor and oven, as described in the literature. The proposed synthesis was conducted with a heating system under reflux … Show more

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