In this paper, the reverse flow in a square duct with an obstruction at the front (which is a square plate), is investigated using particle image velocimetry (PIV). The gap g between the obstruction and the entry to the duct was systematically varied, and it was found that maximum reverse flow occurs around a g/w value of 0.75. The velocity vectors, vorticity plots, and other details described indicate that the flow field is different compared with the two-dimensional channel case.