1986
DOI: 10.1016/0033-0655(86)80003-6
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Resinous polymer analyses using chemical cleavage and chromatography

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Cited by 5 publications
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“…In the IUPAC method the carboxylic acids are determined by gas chromatography after transesterification with lithium methoxide; the polyols are determined by gas chromatography after aminolysis and acetylation [516]. Chemical workup methods (e.g., hydrolysis with alcoholic alkali, alkali fusion, aminolysis with hydrazine, and transesterification with sodium methoxide) for various resins are described in [517]. Alkaline hydrolysis has the disadvantage that it results in low fractions for polyunsaturated fatty acids and lower polyols.…”
Section: Analysis Of Bindersmentioning
confidence: 99%
“…In the IUPAC method the carboxylic acids are determined by gas chromatography after transesterification with lithium methoxide; the polyols are determined by gas chromatography after aminolysis and acetylation [516]. Chemical workup methods (e.g., hydrolysis with alcoholic alkali, alkali fusion, aminolysis with hydrazine, and transesterification with sodium methoxide) for various resins are described in [517]. Alkaline hydrolysis has the disadvantage that it results in low fractions for polyunsaturated fatty acids and lower polyols.…”
Section: Analysis Of Bindersmentioning
confidence: 99%