“…Hydrogen peroxide (H 2 O 2 ), as a vital reactive oxygen species, creates a wide demand for effective concentration monitoring in pharmaceutical, environmental, and food manufacturing areas, which is generated from certain classic biochemical reactions catalyzed by enzymes. − Therefore, it is urgent to develop a stable and precise detector to characterize the amount of H 2 O 2 , ranging from disease prevention to improvement in the quality of daily life. − Recently, some conventional techniques for H 2 O 2 determination have been reported, including fluorescence, spectrophotometry, and electrochemistry. − Among these traditional ways, the electrochemical method attracts great attention due to its rapid response, high sensitivity, and simple instruments . Under the potential scan conditions, H 2 O 2 can be directly oxidized or reduced on the surface of electrochemically active solid electrodes, while these processes are often confined by slow electrode kinetics in multistep chemical reactions and high overpotential, which will influence the sensing performances and trigger interferences from other existing electroactive species at the same time. − Currently, some research studies on the electrochemical detection of H 2 O 2 are mainly focused on electrode modification to promote the electron transfer and simultaneously decrease the electrode polarization . Up to date, various nanostructured materials have been introduced into electrode modification for acquiring the desirable chemical, physical, and electronic properties, including exfoliated graphitic carbon nitride/ZnO nanosheets, nanostructured ZnO thin films, Pt-SWCNT network films, etc. − As a novel two-dimensional (2D) semiconductor material, graphitic carbon nitride (g-C 3 N 4 ) has attracted abundant interest in the electrocatalysis field .…”