Abstract:Source of materialThetitle compound was obtained commercially (Fluka).Crystals suitable for the diffraction study were obtained upon recrystallizationfromwater.
Experimental detailsCarbon-bound Hatoms were placed in calculated positions(C-H 0.95 Åfor aromatic carbon atomsand C-H0.99Åfor methylene groups) and were included in the refinement in the riding model approximation, with U iso (H) setto1.2U eq (C). The Hatoms of the methyl groups were allowed to rotate with afixed angle around the C-C bond to best fit … Show more
“…Furthermore, the benefit of choosing the adequate size of counterions to crystallize ionic compounds has been confirmed on many occasions [12]. In continuation of our interest in metrical features of large cations [13][14][15] the title structure has been determined. Furthermore, the molecular and crystal structure of metaphenylene diamine has been determined earlier [16].…”
“…Furthermore, the benefit of choosing the adequate size of counterions to crystallize ionic compounds has been confirmed on many occasions [12]. In continuation of our interest in metrical features of large cations [13][14][15] the title structure has been determined. Furthermore, the molecular and crystal structure of metaphenylene diamine has been determined earlier [16].…”
“…Furthermore, the benefit of chosing the adequate size of counterions to crystallize ionic compounds has been confirmed on many occasions [12]. In continuation of our interest in metrical features of large cations [13][14][15] the structure of the title compound has been determined. Methacholine chloride is a synthetic derivative of acetylcholine, a neurotransmitter.…”
“…Furthermore, the benefit of choosing the adequate size of counterions to crystallize ionic compounds has been confirmed on many occasions [12]. In continuation of our interest in metrical features of large cations [13][14][15] the structure of the title compound has been determined. A comparable molecular connectivity pattern has been characterized structurally previously in form of the chloride [16] and perchlorate [17] salts of 4-chloro quinuclidinium.…”
C6H13Cl2N, orthorhombic, P212121 (no. 19), a = 6.0087(3) Å, b = 10.1176(6) Å, c = 14.3532(7) Å, V = 872.58(8) Å3, Z = 4, Rgt(F) = 0.0304, wRref(F2) = 0.0632, T = 200 K.
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