Abstract:Carboxyl-14G-10-formyldecanoic acid was made by 14C02 carbonation of 10-undecenylmagnesium bromide and ozonolysis of the product. Attempts were made to equilibrate its methyl ester with CHz / \ @R(CM2)gCOOMe and CH2 GH(CH2)8COOMe in various solvents. Little in-'0-0' corporation of label in the re-isolated ozonide was found, and it was concluded that under normal ozonolysis conditions the formation of ring ozonide is essentially irreversible. Slight incorporation in chloroform is explicable either by reversal o… Show more
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