Reaction monitoring via benchtop nuclear magnetic resonance spectroscopy: A practical comparison of on‐line stopped‐flow and continuous‐flow sampling methods
Tristan Maschmeyer,
David J. Russell,
José G. Napolitano
et al.
Abstract:The ability for nuclear magnetic resonance (NMR) spectroscopy to provide quantitative, structurally rich information makes this spectroscopic technique an attractive reaction monitoring tool. The practicality of NMR for this type of analysis has only increased in the recent years with the influx of commercially available benchtop NMR instruments and compatible flow systems. In this study, we aim to compare 19F NMR reaction profiles acquired under both on‐line continuous‐flow and stopped‐flow sampling methods, … Show more
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