Pyrohydrolytic separation of fluoride and chloride in U–Zr and U–Pu–Zr metallic fuel alloys through oxidation accompanied by estimation using ion chromatography

Bootharajan, M.; Hemalatha, V.; Vithya, J.; Saha, Debasish; Jain, Ashish; Ramanathan, N.; Sundararajan, K.

doi:10.1007/s10967-023-09156-0

J Radioanal Nucl Chem

2023

DOI: 10.1007/s10967-023-09156-0

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Pyrohydrolytic separation of fluoride and chloride in U–Zr and U–Pu–Zr metallic fuel alloys through oxidation accompanied by estimation using ion chromatography

M. Bootharajan,

V. Hemalatha,

J. Vithya

et al.

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Cited by 3 publications

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Comprehensive review of combustion ion chromatography for the analysis of total, adsorbable, and extractable organic fluorine

Shelor,

Warren,

Odinaka

et al. 2024

J of Separation Science

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Poly‐ and perfluoroalkyl substances (PFAS) are a class of persistent organic pollutants whose high stability and appreciable water solubility have led to near‐global contamination. PFAS are bioaccumulative toxins that have been linked to a myriad of disorders and have been detected nearly universally in human blood. Liquid chromatography‐tandem mass spectrometry is the most frequent method used for quantitation, though this typically only measures a few dozen of the >14 000 known PFAS and has been shown to account for a small portion of the total organic fluorine present. Sum parameter methods such as total, extractable, and adsorbable organic fluorine have emerged as alternative measurements for PFAS determination. Combustion ion chromatography has become the preferred method for organofluorine measurement where the sorbent or extract containing PFAS is combusted and the emitted hydrofluoric acid (HF) is a measure of the cumulative organofluorine present. Herein we critically review the types of organofluorine measurement, their separation from the sample matrix, and key parameters of the analytical instrument that affect sensitivity, reproducibility, and recovery with regards to PFAS analysis.

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Comprehensive review of combustion ion chromatography for the analysis of total, adsorbable, and extractable organic fluorine

Shelor,

Warren,

Odinaka

et al. 2024

J of Separation Science

View full text Add to dashboard Cite

show abstract

Determination of chemical elements and natural radionuclides in shopping plastic bags using k0-neutron activation analysis

Al-Ghamdi,

Mohery,

Soliman

2023

J Radioanal Nucl Chem

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Rapid separation, purification of 90Sr and feasibility studies for the preparation of 90Y resin microsphere brachytherapy source from FBTR irradiated fuel dissolver solution

Saha,

Vithya,

Kalaiarasu

et al. 2024

J Radioanal Nucl Chem

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Pyrohydrolytic separation of fluoride and chloride in U–Zr and U–Pu–Zr metallic fuel alloys through oxidation accompanied by estimation using ion chromatography

Cited by 3 publications

References 22 publications

Comprehensive review of combustion ion chromatography for the analysis of total, adsorbable, and extractable organic fluorine

Comprehensive review of combustion ion chromatography for the analysis of total, adsorbable, and extractable organic fluorine

Determination of chemical elements and natural radionuclides in shopping plastic bags using k0-neutron activation analysis

Rapid separation, purification of 90Sr and feasibility studies for the preparation of 90Y resin microsphere brachytherapy source from FBTR irradiated fuel dissolver solution

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