“…These samples were either from (1) material produced in the conversion prototype 7 (HFIR-2, HFIR-3) or (2) materials prepared at ORNL for the water sorption studies as described in Sect. 2.1.1 (HFIR-4, HFIR-5, HFIR-6-1, HFIR-6-2, HFIR-6-3).…”
Section: Materials Irradiatedmentioning
confidence: 99%
“…3, significant water loss (0.97/1.6) occurred on drying overnight at 120ºC and all of the adsorbed moisture was removed after holding at 650ºC for 24 h. (Note the difference between the 150ºC temperature for the major water removal from U 3 O 8 and that of 400ºC for UO 3 -which is due, in the latter, to the necessity to decompose the uranyl dihydroxide bonds shown in Eq. [7].) Higher temperatures are unnecessary.…”
“…These samples were either from (1) material produced in the conversion prototype 7 (HFIR-2, HFIR-3) or (2) materials prepared at ORNL for the water sorption studies as described in Sect. 2.1.1 (HFIR-4, HFIR-5, HFIR-6-1, HFIR-6-2, HFIR-6-3).…”
Section: Materials Irradiatedmentioning
confidence: 99%
“…3, significant water loss (0.97/1.6) occurred on drying overnight at 120ºC and all of the adsorbed moisture was removed after holding at 650ºC for 24 h. (Note the difference between the 150ºC temperature for the major water removal from U 3 O 8 and that of 400ºC for UO 3 -which is due, in the latter, to the necessity to decompose the uranyl dihydroxide bonds shown in Eq. [7].) Higher temperatures are unnecessary.…”
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