Process Development and Characterization of 2-Aminopyridine Potassium Dihydrogen Orthophosphate (2APKDP) Crystal

Sivavishnu, D.; Srineevasan, R.; Johnson, J.

doi:10.26438/ijsrpas/v7i3.2733

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Fourier Transforms Infrared Spectroscopy (Ftir)1

B X-ray Diffraction1

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2019

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“…By interpreting the infrared absorption spectrum of the compound shows that a band in the region 3217-3230 cm -1 due to (N-H stretching). Similarly band in the region 1740-1685 cm -1 due to (C=O stretching), 1240-1270 cm -1 due to (C-O stretching) and 785-775 cm -1 due to (C-Cl stretching) [8][9].…”

Section: Fourier Transforms Infrared Spectroscopy (Ftir)mentioning

confidence: 91%

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Synthesis and Characterization Of Diethyl 4-Amino-1-(3-Chlorophenyl)-1H-Pyrazole-3,5 Dicarboxylate

Jain¹,

Mishra²

2019

IJSRPAS

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In the present study, Diethyl 4-amino-1-(3-chlorophenyl) -1H-pyrazole-3,5 dicarboxylate (D4A1(3-cl)1HP35D) was synthesized. The structure of newly synthesized compounds of Diethyl 4-amino-1-(3-chlorophenyl -1H-pyrazole-3,5 dicarboxylate was characterized by x-ray diffraction (XRD), Fourier transforms infrared spectroscopy (FTIR) and Transmission electron microscopy (TEM). The compound has been prepared by the chemical root method and crystal structure was determined by x-ray diffraction technique. The XRD pattern of (D4A1(3-cl)1HP35D) confirms the crystalline nature and (h k l) values are indexed. From the experimental analysis, the presence of functional groups in the synthesized compound and particle size of the compound has been estimated by FTIR and TEM spectroscopy.

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Section: Fourier Transforms Infrared Spectroscopy (Ftir)mentioning

confidence: 91%

“…The compound has monoclinic crystal lattice with unit cell volume V = 892.10 × 10-8 cm3. The unit cell parameters are a = 13.92 Ǻ, b = 6.68 Ǻ, c = 9.64 Ǻ, and β= 94.60˚ [8]. Inter-planar d spacing and unit cell volume of the synthesized compound was calculated by the formula: And volume is given by V = abc…”

Section: B X-ray Diffractionmentioning

confidence: 99%

Synthesis and Characterization Of Diethyl 4-Amino-1-(3-Chlorophenyl)-1H-Pyrazole-3,5 Dicarboxylate

Jain¹,

Mishra²

2019

IJSRPAS

View full text Add to dashboard Cite

show abstract

Process Development and Characterization of 2-Aminopyridine Potassium Dihydrogen Orthophosphate (2APKDP) Crystal

Cited by 1 publication

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Synthesis and Characterization Of Diethyl 4-Amino-1-(3-Chlorophenyl)-1H-Pyrazole-3,5 Dicarboxylate

Synthesis and Characterization Of Diethyl 4-Amino-1-(3-Chlorophenyl)-1H-Pyrazole-3,5 Dicarboxylate

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