1964
DOI: 10.1007/bf00846494
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Procedure in the synthesis of ethyllithium in an atmosphere of argon

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“…IR spectra were recorded as paraffin mull between KBr plates with a Shimadzu Prestige 21 spectrometer; electron impact mass spectra with a Varian mass spectrometer. 1,3-(H-CϵC) 2 C 6 H 4 , HSiEt 3 , Ph 2 MeSiCl and PhMe 2 SiCl are commercially available, EtLi [26] and Cl 2 GaH [6] were synthesised according to reported procedures.…”
Section: Methodsmentioning
confidence: 99%
“…IR spectra were recorded as paraffin mull between KBr plates with a Shimadzu Prestige 21 spectrometer; electron impact mass spectra with a Varian mass spectrometer. 1,3-(H-CϵC) 2 C 6 H 4 , HSiEt 3 , Ph 2 MeSiCl and PhMe 2 SiCl are commercially available, EtLi [26] and Cl 2 GaH [6] were synthesised according to reported procedures.…”
Section: Methodsmentioning
confidence: 99%