Preparation of Mg(OH)2 Nanorods

Li, Y.; Sui, Meirong; Ding, Yue; Zhang, G.; Zhuang, Jin; Wang, C.

doi:10.1002/(sici)1521-4095(200006)12:11<818::aid-adma818>3.0.co;2-l

Cited by 217 publications

(128 citation statements)

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“…One of the most popular synthesis techniques in the literatures is through the hydrolysis of titanium alkoxide in water followed by either thermal [32][33][34] or hydrothermal treatment [35][36][37][38][39][40]. Hydrothermal synthesis is directly carried out at high temperatures, but the resulting nanocrystals are rather agglomerated and the process involves high pressure [25].…”

Section: Introductionmentioning

confidence: 99%

Room temperature synthesis of titania microspheres by hydrolysis of titanium alkoxide using water vapor

Wang

Chen

et al. 2006

Journal of Alloys and Compounds

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Section: Introductionmentioning

confidence: 99%

Room temperature synthesis of titania microspheres by hydrolysis of titanium alkoxide using water vapor

Wang

Chen

et al. 2006

Journal of Alloys and Compounds

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“…However, elevated temperatures and pressure are the key factors that kinetically facilitate the decomposition and formation of Mg(OH) 2 nuclei. The earlier techniques involving hydrothermal hydrolysis to produce Mg(OH) 2 and subsequent thermal decomposition to obtain MgO nanorods has been well explained [18].…”

Section: 4mentioning

confidence: 99%

Fabrication of magnesium hydroxide nanoneedles

Al-Owais

El‐Mossalamy

Shah

et al. 2011

Chem Technol Fuels Oils

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Magnesium hydroxide Mg(OH) 2 nanoneedles with diameters of 40-60 nm and lengths of more t h a n 6 5 0 n m h a v e b e e n f a b r i c a t e d b y a f a s t a n d s a f e ro u t e i n d e -i o n i z e d w a t e r. X -r a y diffraction (XRD) showed that the Mg(OH) 2 nanoneedles were well-crystallized with the hexagonal structure, whereas from the morphological investigations using scanning electron microscope (SEM), it was revealed that the nanoneedles are grown in a very high density over the whole foil substrate. The structure features were also analyzed by high~resolution transmission electron microscopy (TEM). The approach is based on a simple reaction of magnesium foil and de-ionized water without using surfactants.The reaction time is 3 h and the temperature is ~110°C. The advantages of producing nanoneedles using this method include ease, flexibility, speed, and cost. The process can easily be scaled up.

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“…This process occurring for the plates eventually led to the formation of rods. Several reports implied that the nanoplate is a substable state for hexagonal structured crystals [21][22][23]. They regarded rolling as the mechanism for the conversion from plates to rods.…”

Section: Growth Mechanismmentioning

confidence: 99%