Zaini b), c) , Yoshimasa Amano d), e) and Motoi Machida d), e), * Activated carbons were prepared by activating oil palm empty fruit bunches (EFB) using various chemicals including H 3 PO 4 , KOH or ZnCl 2 and were characterized by elemental analysis, nitrogen and methylene blue adsorption. The effect of the pretreatment of EFB by NaOH was also investigated. Among all samples, EFB pre-washed with NaOH and then activated with ZnCl 2 showed the greatest maximum adsorption capacity (357 mg/g) and BET specific surface area (1265 m 2 /g). The experimental data of all adsorbents were well fitted to the Langmuir isotherm model and pseudo-second-order kinetics model. This study demonstrated that ZnCl 2 activation was the best way to obtain an activated carbon, and that NaOH pre-washing was effective as well for developing mesopores in EFB activated by H 3 PO 4 and ZnCl 2 .