2000
DOI: 10.1016/s0254-0584(00)00238-8
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Preparation and characterization of strontium zirconate (SrZrO3) fine powders

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Cited by 31 publications
(12 citation statements)
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“…3) indicates that there is an inverse relationship between aging temperature and aging time. As reported in other studies [15,19], high temperature accelerates the formation of large crystals; thus at high temperature fewer grains are formed, allowing an orderly growth (nucleation process). According to Rinaldi [20], during aging, particles of aluminum hydroxide are solubilized and growth take place through condensation reactions; this growing process can be accelerated at high temperatures, leading to the formation of particles of large size.…”
Section: Resultssupporting
confidence: 54%
See 1 more Smart Citation
“…3) indicates that there is an inverse relationship between aging temperature and aging time. As reported in other studies [15,19], high temperature accelerates the formation of large crystals; thus at high temperature fewer grains are formed, allowing an orderly growth (nucleation process). According to Rinaldi [20], during aging, particles of aluminum hydroxide are solubilized and growth take place through condensation reactions; this growing process can be accelerated at high temperatures, leading to the formation of particles of large size.…”
Section: Resultssupporting
confidence: 54%
“…The peak located at 761 cm −1 is assigned to the tetrahedral coordination AlO 4 [15]. The anion [Al(OH) 4 ] − is found at high pH and absorbs at 615 cm −1 [14].…”
Section: Resultsmentioning
confidence: 99%
“…At this temperature all the reflections match with the reported orthorhombic structure of the SZO phase [20]. As a conclusion, the SZO formation take place in two steps, it starts around 650 • C and the pure phase is obtained at 900 • C. The same observations were evidenced when oxalates were used as precursors [21,22].…”
Section: Strontium Zirconate Precursor Powder Characterizationsupporting
confidence: 81%
“…Several methods have been reported to prepare SrZrO 3 powders: conventional solid state reaction of SrCO 3 and ZrO 2 , coprecipitation, hydrothermal [7], sol-gel [8], and a method using single molecular (strontium zirconyl oxalate) precipitate as precursor [9]. In order to get homogeneous SrZrO 3 nanocrystals, the present study adopted a sol-gel combustion method, and introduced citric acid as chelator in the synthesis process and as fuel during the combustion process [10].…”
Section: Introductionmentioning
confidence: 99%