“…The nitrogen component will be minor in unmodified fibers with sp 2 carbon being the predominant species and, it is the oxidative destruction of the latter that gives rise to the carbon-oxygen functionality. A large number of treatment options have been pursued [19], such as electrochemical oxidation (anodisation) which is well established as an effective technique for the generation of oxygen functional groups as well as enabling the etching of the surface [8,[26][27][28]. It is now commonplace for carbon fiber electrodes, whether discrete fibers, bundles, mats or cloths, to be electrochemically treated prior to further application in order to improve electron transfer kinetics [11,12,28].…”