Preparation and Absorption Spectra of Some β-Aryl-α-Mercaptoacrylic Acids and Related Disulfides<sup>1,2</sup>

Campaigne, E.; Cline, Richard E.

doi:10.1021/jo01107a006

Cited by 78 publications

(32 citation statements)

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“…8 Triphenyltin hydroxide (Aldrich-Chemie) and diisopropylamine (Merck) were used as supplied. Diisopropylammonium hydrochloride was prepared by addition of HCl to an aqueous solution of diisopropylamine.…”

Section: Methodsmentioning

confidence: 99%

Triphenyltin(IV) sulfanylpropenoates: synthesis, crystal structures and antimicrobial activities

Casas

Castiñeiras²,

Couce

et al. 2000

Appl. Organometal. Chem.

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Three new triphenyltin(IV) sulfanylcarboxylates with the general formula [Q][SnPh 3 (L)] (Q = diisopropylammonium cation; L = tspa, pspa or pyspa, where t = 3-(2-thienyl)-, p = 3-(2-phenyl)-, py = 3-(2-pyridinyl)-and spa = 2-sulfanylpropenoato) have been prepared by reaction of triphenyltin(IV) hydroxide with the corresponding acid in the presence of di-isopropylamine in ethanol. The compounds have been characterized by elemental analysis and mass spectrometry and by IR, Mössbauer and NMR ( 1 H, 13 C, 119 Sn) spectroscopy. X-ray studies of the crystal structures of [Q][SnPh 3 (pspa)] and [Q][SnPh 3 (pyspa)] show that in both compoundsthe tin atom is coordinated to three phenyl C atoms and to S and one O atom of the ligand L. All three complexes are active against strains of the Gram-positive bacterium Staphylococcus aureus, but are inactive or only slightly active against the Gram-negative bacteria Escherichia coli and Pseudomonas aeruginosa.

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Section: Methodsmentioning

confidence: 99%

Triphenyltin(IV) sulfanylpropenoates: synthesis, crystal structures and antimicrobial activities

Casas

Castiñeiras²,

Couce

et al. 2000

Appl. Organometal. Chem.

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“…The 3-(aryl)-2-sulfanylpropenoic acids were prepared [19] by condensation of the appropriate aldehyde with rhodanine (Rhod), subsequent hydrolysis in an alkaline medium of the Rhod derivative and acidification with aqueous HCl. Specific experimental conditions for H 2 pspa, H 2 fspa and H 2 tspa were described in Ref.…”

Section: Synthesismentioning

confidence: 99%

Synthesis, structure and cytotoxicity of triphenylphosphinegold(I) sulfanylpropenoates

Barreiro

Casas

Couce

et al. 2008

Journal of Inorganic Biochemistry

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“…The starting compounds 1a-c [27] and hydrazonyl chlorides 2a-c [28] were prepared according to published procedures.…”

Section: Methodsmentioning

confidence: 99%

Facile synthesis of new (Z)-6-arylmethylidene-1,3,4-thiadiazin-5(6H)-one derivatives

Metwally

Abdelrazek

Jaeger

2013

Chem Heterocycl Comp

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Preparation and Absorption Spectra of Some β-Aryl-α-Mercaptoacrylic Acids and Related Disulfides^1,2

Cited by 78 publications

References 0 publications

Triphenyltin(IV) sulfanylpropenoates: synthesis, crystal structures and antimicrobial activities

Triphenyltin(IV) sulfanylpropenoates: synthesis, crystal structures and antimicrobial activities

Synthesis, structure and cytotoxicity of triphenylphosphinegold(I) sulfanylpropenoates

Facile synthesis of new (Z)-6-arylmethylidene-1,3,4-thiadiazin-5(6H)-one derivatives

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Preparation and Absorption Spectra of Some β-Aryl-α-Mercaptoacrylic Acids and Related Disulfides1,2

Cited by 78 publications

References 0 publications

Triphenyltin(IV) sulfanylpropenoates: synthesis, crystal structures and antimicrobial activities

Triphenyltin(IV) sulfanylpropenoates: synthesis, crystal structures and antimicrobial activities

Synthesis, structure and cytotoxicity of triphenylphosphinegold(I) sulfanylpropenoates

Facile synthesis of new (Z)-6-arylmethylidene-1,3,4-thiadiazin-5(6H)-one derivatives

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Preparation and Absorption Spectra of Some β-Aryl-α-Mercaptoacrylic Acids and Related Disulfides^1,2