Predictive Analytics and Risk Assessment: A Logical Response to Intimate Partner Homicide

Ross, Lee E.

doi:10.25141/2576-3563-2017-1.0001

IJCF

2017

DOI: 10.25141/2576-3563-2017-1.0001

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Predictive Analytics and Risk Assessment: A Logical Response to Intimate Partner Homicide

Lee E. Ross¹

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2024

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A new fluorescence probe for sofosbuvir analysis in dosage form and spiked human plasma

Nasr,

Talaat,

Morshedy

et al. 2024

Luminescence

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A simple, rapid, and low‐cost technique was developed to allow reliable analysis of the anti‐hepatitis C drug sofosbuvir in bulk, tablet form, and spiked human plasma. This method depends on the ability of sofosbuvir to quench the fluorescence of the newly synthesized 2‐amino‐3‐cyano‐4,6‐dimethylpyridine (reagent 3). Elemental analysis and spectral data were used to validate the structure of the synthesized reagent. The newly synthesized reagent exhibited a satisfactory level of fluorescence emission at 365 nm after excitation at 247 nm. All experimental variables that might affect the quenching process were analyzed and optimized. Linearity, range, accuracy, precision, limit of detection (LOD), and limit of quantitation (LOQ) were all validated in accordance with the International Council for Harmonization of Technical Requirements for Pharmaceuticals for Human Use (ICH) guidelines. The concentration range was shown to be linear between 0.1 and 1.5 μg/mL. The technique was effectively utilized for sofosbuvir analysis in both its tablet dosage form and spiked human plasma, with mean percentage recoveries of 100.13 ± 0.35 and 94.26 ± 1.69, respectively.

show abstract

A new fluorescence probe for sofosbuvir analysis in dosage form and spiked human plasma

Nasr,

Talaat,

Morshedy

et al. 2024

Luminescence

View full text Add to dashboard Cite

show abstract

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Predictive Analytics and Risk Assessment: A Logical Response to Intimate Partner Homicide

Cited by 1 publication

References 8 publications

A new fluorescence probe for sofosbuvir analysis in dosage form and spiked human plasma

A new fluorescence probe for sofosbuvir analysis in dosage form and spiked human plasma

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