Precision of the Microelectrolytic Determination of Copper

MacNevin, W. M.; Bournique, Raymond A.

doi:10.1021/ac50147a023

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1942

1961

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Cited by 4 publications

(2 citation statements)

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“…After the method was developed it was tested with fifteen samples of cast iron or steel containing varying amounts of copper. These samples are described in (7) on the precision of the microelectrolytic determination of copper. In doing so the Pregl and Hermance-Clarke (1) electrolytic cells were compared.…”

Section: Samplesmentioning

confidence: 99%

Determination of Copper in Cast Iron by Direct Microelectrolysis

MacNevin¹,

Bournique²

1943

Ind. Eng. Chem. Anal. Ed.

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Section: Samplesmentioning

confidence: 99%

Determination of Copper in Cast Iron by Direct Microelectrolysis

MacNevin¹,

Bournique²

1943

Ind. Eng. Chem. Anal. Ed.

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“…While the determination of a cooling curve is considered the best method of establishing the purity of a solid organic compound, it is seldom used because it requires several grams of the sample. The recent publication of a method (316) using only 200 to 300 mg. should make this excellent procedure of more general application. The material contained in a special glass tube is placed in a copper block and heated so that a constant difference in temperature is maintained between the sample and its surroundings.…”

Section: Melting Pointmentioning

confidence: 99%