2003
DOI: 10.1023/a:1020759618262
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Cited by 11 publications
(3 citation statements)
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“…We also added a small amount of a-aV-azobutyronitrile (98% purity, Fluka Chemical, Buchs, Switzerland) as a thermochemical initiator. The quantities used here were optimized in a previous study [12]. Polymerization and, consequently, gel formation, occurs within a few seconds, when the temperature reaches 80 jC, approximately.…”
Section: Preparationmentioning
confidence: 99%
“…We also added a small amount of a-aV-azobutyronitrile (98% purity, Fluka Chemical, Buchs, Switzerland) as a thermochemical initiator. The quantities used here were optimized in a previous study [12]. Polymerization and, consequently, gel formation, occurs within a few seconds, when the temperature reaches 80 jC, approximately.…”
Section: Preparationmentioning
confidence: 99%
“…The resulting powders show a homogeneous grain size distribution in the nanometer range [43]. This synthesis method is fast, clean and easy to reproduce with the advantage of a reduction in the temperature to complete the chemical reaction [44][45][46][47][48]. Recently, this method was used to control the grain size homogeneity [49] and which also improve thermoelectric properties of samples [50].…”
Section: Introductionmentioning
confidence: 99%
“…In this paper, ZrO 2 :10 mol% Sc 2 O 3 nanosize powders were synthesized by the polyacrylamide (18,19) and the polymeric precursor (20) techniques. Details of the syntheses have already been presented (21).…”
Section: Introductionmentioning
confidence: 99%