1976
DOI: 10.1002/pssa.2210340239
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Positron annihilation investigation for an estimation of the dislocation density and vacancy concentration of plastically deformed polycrystalline Ni of different purity

Abstract: From the angular correlation measurements of the positron annihilation radiation on cold rolled, polycrystalline Ni of purity 99.99% and 99.84% the curve‐shape parameters S are determined for treating the as‐deformed and annealed samples up to a thickness reduction of 90%. The trapping rate of the positrons can be determined for a thickness reduction up to 15 or 18% for the dislocations and for the vacancies as well. Using known relations for the hardening within range 2 the specific trapping rates are estimat… Show more

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Cited by 80 publications
(22 citation statements)
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“…An agreement between σ w and S/W confirms that residual stresses origin is an increase in defect density. Analogous rise of S parameter was observed for cold rolled nickel [14]. In this case the saturation of S value was explained as positron trapping in vacancies only.…”
Section: Resultssupporting
confidence: 71%
“…An agreement between σ w and S/W confirms that residual stresses origin is an increase in defect density. Analogous rise of S parameter was observed for cold rolled nickel [14]. In this case the saturation of S value was explained as positron trapping in vacancies only.…”
Section: Resultssupporting
confidence: 71%
“…Then, the mean lifetime saturates at the value about 210 ps. This is characteristic feature, occurring for instance for Ni [14], Cu [15] and also other metals exposed to the compression. The saturation can be explained by so large defect concentration, usually about 10 3 , that after termalization all positrons are trapped at open volume defects where they annihilate.…”
Section: The Sample Exposed To Compression the Calibration Testmentioning
confidence: 89%
“…where k f is the positron annihilation rate in the bulk (free) state; l v is the specific positron trapping rate into defects (for monovacancies in Ni l v = 2.2 Â 10 15 s À1 [19]); S f and S v are the S-parameters characteristic of the positron annihilation from the bulk (free) and monovacancy-trapped states, respectively. The value S f = 0.520 ± 0.001.…”
Section: Methodsmentioning
confidence: 99%